GCMS analysis results for sample AE10020, May 2002

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Laboratory report documenting GCMS analysis of sample AE10020 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044132–000044143

Folder label: “GCMS X 4/26/02 A 5/8/02”

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NYC 9/11 Public Portal Document

. Data File C:\MSDCHEM\1\DATA\020507\10020.D Vial: 19 Acq On 8 May 2002 5:52 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 *****************★*************************************************** Peak Number 5 Phenanthrene-diO Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.33 ug/1 41715 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual V 1 Phenanthrene-diO 188 C14D10 001517-22-2 87 2 Anthracene-d10 - 188 C14D10 001719-06-8 87 3 /H-Naphtho[1,8-bc]thiophen-3-one... 188 C11H8OS 010245-79-1 37 4/1,4-Naphthoquinone, 2,3-dihydro-. . . 188 C12H1202 1000157-22-3 37 Abuidance Scan 4915 (31.958 min): 10020.D (-4905) (-) m/ z 188.20 100.00% 188

5000 94 160 T I 1 1 1 ' i ' 1 ' 1 i ' 'r ' 1 I 1 44 54 66 80 31.60 31.80 32.00 32.20

m/z-> mm Tp 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 108 118 11111111 /1111111111 132 146 m/Z 189.20 28.91%

Abundance #79827: Phenanthrene-d10 188

-..................... ..... 5000 31.60 31.80 32.00 32.20 m/z 94.10 25.87% 80 94 160 30 42 52 66 11 108 118 132 146 11 170179, I... i । । i । i । i iyr t ri | i rn i j i h i 11 m 11 । ■ । 11 । । । । 11 । । । । I I 11 11 r I tttT| H I I |T7 1 I | I | I I [ I I I I | I I | i p-i t I | l iTPI n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1(18 । । r . । । । i-r । -t । । । । . । । । । । 31.60 31.80 32.00 32.20 5000 m/ z 160.00 13.94%

17 30 42 52 e° 80, 94 108 118 132 160 , |. 11" " 11" IT’ 1111111 > 1111111111 mrr 11 ITTT| TTt T 146—.+4179179— n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79735: 3H-Naphtho[1,8-bc]thiophen-3-one, 4,5-dihydro- 1 i ' ■ ' ■ I 1 1 1 1 1J 1 1 1 i r 1 1 1 | 1 188 31.60 31.80 32.00 32.20 m/z 184.10 13.68% 5000 115 160 45 63 TTRT—TRTODaBTgug ‘ i"128 89 145 ■ ' i111' i1 r I I I I [ I I I I I I I r 1’3 171... , ' ।r 1 1 ' i1 1 1 । i1 ' ' ' । 1 > i ' i ' /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10020.D SCAN020507.M Tue May 14 08:44:28 2002 Page 7

NYC-WTC_000044142

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GCMS analysis results for sample AE10025, May 2002 · Box DEP Box 25

NYC-WTC_000044191

Laboratory report documenting GCMS analysis of sample AE10025 conducted on May 14, 2002, identifying unknown compounds.

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