GCMS analysis results for sample AE10022, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\020507\10022 . D Vial: 21 Acq On 8 May 2002 7:50 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 IH-Cyclopropa[1]phenanthren... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.32 ug/1 42005 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 IH-Cydlopropa[1]phenanthrene,la,... 192 C15H12 000949-41-7 50 2 Naphtho[2,3-b]norbornadiene 192 C15H12 1000210-52-3 50 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 4 Anthracene, 2-methyl-_______________ 192 C15H12 000613-12-7 50 Abundance / Scan 4767 (31.088 min): 10022.D (-4757) (-) m/z 192.10 100.00% 19 2

5000 146 ..... 4.3....... 40 51 70 82 96 134 160 30.80 31.00 31.20 31.40 ■ । 1 " ' । 1 ■ " I " 1 ■ i'1 1 । ’ 1 1 1 I " 1 1 । ■I...... ......... ■ r 1" i " " r' ‘ ■ i1 ‘HT* ! Il | I I I I | I I ! I | I —H - m/z 146.10 31.52% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81038:1H-Cyclopropa[l]phenanthrene,1a,9b-dihydro- 192

5000 30.80 31.00 31.20 31.40 165 m/z 193.20 19.53% 27 39 51 63 74 83 96 105 115 126 139 152 | 176 ' I " " I 1 1 ' 'T1'1 ' ' I' ‘ I 1 lri F’s । I I i p । । । >'i । । । . i . । , i r i'| i i n-fl-i i i I । i i II । i I i1!1 Tyur n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81026: Naphtho[2,3-b]norbornadiene 192

30.80 31.00 31.20 31.40 5000 m/z 191.00 14.95% 165

m/z-> 39 51 63 73 82 96 105 115 126 1111 ■ ■ i11 "'i11111'''111111 "M‘ F..... ..... 9 11 > 111 "t’i 11 < 111111 n'l 11 ri |*i'i 11 pTh । TTTTTN 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 139 152 1 176 4 Abundance #81033: Phenanthrene, 9-methyl- A..... 1 1 1 1 1 1 1 1 I 11 11 1 A 192 30.80 31.00 31.20 31.40 m/z 82.00 11.36%

5000

... 1 .k... 96 115 126 139 152 165 176 , I 29 39 51 63 74 83 J ‘ I | i i i < | i i ■ r । r I r i |i i i I | 111 I I J r I'r 'I |'I I I’ll I I I I | i " " i " । "i " 1 Ttrri 1‘t‘ r| । rl । rli TTp-r 1 1 i ■ ■ ‘ ' i 1 1 1 1 11 1 1 1 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

10022.D SCAN020507.M Tue May 14 08:45:17 2002 Page 4

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