GCMS analysis results for sample AE10022, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\020507\10022.D Vial: 21 Acq On 8 May 2002 7:50 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.35 ug/1 45364 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 90 2 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 53 3 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 50 4 2 ,2,9,9-Tetramethyldec-5-ene-3 ,7... 188 C14H20 102745-35-7 49 Abundance Scan 4914 (31.952 min): 10022.D (-4907) (-) m/z 188.20 100.00% 188

5000 ■ • I r 1 ' — । ।T | i । । i | । । । i | ।

RR 80 94 160 31.60 31.80 32.00 32.20 36 44 66 H | 104 132 145 . 172 n 11 । i i i i । । i i i । i i t i p f i i । I i i r i I 11 । i rl I । < '> i i j ) I > i । i /1 i '| 1 i >> । > i i i p i-:- Ci > । i i 1 1'[ I i < i | I i r r| i I TTTr m/z 184.20 17.22% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 93.95 16.45% 80 94 160 1 17 30 42 52 ° , J 108 118 132 146 I 1701791, TTngui । fl 11 [ t i 111 I I 11 I'i I I i ]'i i I 11 I 11 11 I h i 11 i 11 [ i i 11 । FT |li t ITTTfTTT i IT|'i 11 i pvn t 4rr T’T /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl 188 "I ' I r ‘‘ ' I 1 l i 3 I “I 11 I I I • I I I I 31.60 31.80 32.00 32.20 5000 m/z 189.20 12.93% 79 __ . 159 173 145 107 119 131 ।| । 91I z-> ' i11'1 r ‘1' i' ■ " r ' " i" " i TT IT' 1 II’ ""If- 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 44 Abundance #79722: Cyclohexanone, phenylhydrazone 188 31.60 31.80 32.00 32.20 93 m/z 160.10 12.43%

5000 55 65 41 77 106 145 । i29 120 132 'i'i 11,11 ।, Irl , । .-I H 11 m ।, i1 II 159 170 11 ‘ ‘* 11 ------- TTT 11'' 'I''1'11111111 ^TTTT 1 1 i r. ' - । । । 11 । , , > , । । । । । । । m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10022.D SCAN020507.M Tue May 14 08:45:19 2002 Page 5

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