GCMS analysis results for sample AE10702, May 20 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\020513\10702.D Vial: 13 Acq On : 14 May 2002 12:24 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 8 Anthracene-dlO- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.36 ug/1 44214 Phenanthrene-dl0 31.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

l Anthracene-dl0- 188 C14D10 001719-06-8 87 2 Phenanthrene-d10 188 C14D10 001517-22-2 68 3 Cycloheptanone, 4-phenyl- 18 8 C13H160 067688-28-2 43 4 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 37 Abundance Scan 4915 (31.958 min): 10702. D (-4905) (-) m/z 188.15 100.00% 188

5000 ./ 4 1 IT | 1 1 । । | ' । । । | ।

94 80 52 66 + ! | !> I I | ! I I ! | I I I I | I I I ' I | 1 I i I | > I । ! | I I I l T 146.150 I I I ■ I > I I I I I I I I I ' I I >> I I I I I I I I I 11 31.60 31.80 32.00 32.20 m/z 184.20 19.53% m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

----------------- । । । । । । । 5000 31.60 31.80 32.00 32.20 m/z .93.90 19.44% — 66 80 । 94। 160

mfe-> 17 30 1 | । h । | . . ' . | 42 52 ' n | I " ' । I ! i > । ,i 1111111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 108 118 132 146 | 179179 11"11

Abundance #79827: Phenanthrene-d10 188 >111, 11d f I I I I I 'I I I I I I 31.60 31.80 32.00 32.20 5000 m/z 189.20 19.06%

80 94 160 30 42 52 66 11 108 118 'i [ I i i I | I । I I p । I । | I 11 r [ trrrtri |TH,I 1 i 1111111111J11111111111111 [ TT 132 64.170179 14 p-trfp-rri-j 11 ri 1’1111 I‘‘ ....‘I lz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- 1 । ।1 1 । । r • 11 । 1 । । 11 1 । । 1 । । 188 31.60 31.80 32.00 32.20 117 104 m/ z 80.10 13.81% 91 160 5000 131 170 27 3i9 51 65 78 145

m/z-> r m 11-i । , 111 I 11 lit । Ip nh i'i L I " 111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 mrill ------------------------- 31.60 31.80 32.00 32.20

10702 .D SCAN020507.M Wed May 15 08:44:10 2002 Page 10

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