GCMS chain of custody form, sample AE10239, May 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020509\10239.D vial: 17 Acq On : 10 May 2002 2:26 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.36 ug/1 49642 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

V1 Anthracene - dl 0 - 188 C14D10 001719-06-8 53 2 1,2 - s (2-hydroxyphenyl) ethylene. . . 376 C24H28N2O2 1000187-13-2 33 3 3,44 Oxazolidinecarboxylic acid, . . . 245 C11H19NO5 116842-10-5 23 4 Sele Abundance nide, ethyl 1-methyl-1-pente... 188 Scan 4913 (31.946 min): 10239.D (-4906) (-) C8H12Se 025128-48-7 9 m/z 188.20 100.00% 188

5000 94 31.60 31.80 32.00 32.20

miz-> 42 TTTTTT 76 +134.140. 320 ■ i111' i "1' i ■ ■" i" " i " " r 1" (" " i " " i" " i" 20 40 60 80 100120 140 160180 200 220 240 260 280 300 320 340 360 380 m/z 94.20 31.55% Abundance #79826: Anthracene-d 10- 188

............................. 5000 31.60 31.80 32.00 32.20 m/z 189.20 23.42% DC 94 160 17 42! 66 J J 114132 1 1 "I ""I'"i l‘i i i ItmTn i rl 11 i‘i rMi 11 i pTi >| 11 TTTTTTTpTTTYTTTTpnTnYnnnYIT^ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79831:1,2-Bis(2-hydroxyphenyl)ethylenediamine, N,N'-bis(... 188

31.60 31.80 32.00 32.20 5000 m/ z 80.20 21.64%

41 77 94 । 121 145 171 । rho 4 P 210 238255 293 377 " r ■" i ■ •" I" 11 r " ‘ i11" i" " I" " r " ' r " ' i" m/z-> 20 40 60 80 100120 140160180 200 220 240 260 280 300 320 340 360 380 Abundance #79684:3,4-Oxazolidinecarboxylic acid, 2-(1,1 -dimethyleth... T*n—mm—TBBBn 188 31.60 31.80 32.00 32.20 m/z 184.05 16.07%

5000

42 88 144 4.4 116 | ,170 , 230 1 rl 11111 rui uph T’IUIUmnmmmpM0CupaT m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 31.60 31.80 32.00 32.20

10239.D SCAN020507.M Tue May 14 14:25:07 2002 Page 5

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