GCMS analysis results for sample AE10208, May 2002

NYC 9/11 Public Portal Document

'Data File C:\MSDCHEM\l\DATA\020509\10208.D Vial: 10 Acq On 9 May 2002 7:31 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.32 ug/1 49344 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

C/L Anthracene-d10- 188 C14D10 001719-06-8 64 V 2 Phenanthrene - d10 188 C14D10 001517-22-2 64 3 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H16O 020758-60-5 33 4 Peptacyclo [7.3.1.1. (4,12) .0(2,7) ... 188 C14H20 1000215-61-8 9 Abundan Scan 4914 (31.952 min): 10208.D (-4906) (-) m/z 188.20 100.00% 188

5000

80 94 ------------------ 160 31.60 31.80 32.00 32.20 52 64 1]0m0m0mtr n 11111"" i" "i" "i "111 I’’ -HH m/z 189.20 23.39% nfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- KB

5000 31.60 31.80 32.00 32.20 m/z 94.10 18.19% 17 30 42 52 66 _ 1 108118 132 146 160 170179/1 11111111 n 11111111i11I11111 11 1111111111111111111111 mri11111 |l i n ।11 H । it Hp ITITINI tHlrrrr n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 KB

31.60 31.80 32.00 32.20 5000 m/z 80.10 18.14%

80 94 160 30 42 52 66 11 108118 132 146 ,|,| 170179,1.1 TITTTTTTTPTTTTTTHTTTHTTTTn /z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79791: Benzene, 1 -(1 -cyclohexen-1 -yl)-4-methoxy- KB 31.60 31.80 32.00 32.20 m/z 184.20 16.57%

5000 160

115 129 145 173 41 51 65 77 91 n/z-> ------- 1924114 frr 4 JU™ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10208.D SCAN020507.M Tue May 14 14:22:34 2002 Page 5

NYC-WTC_000024327