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GCMS analysis results for sample AE10208, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10208 conducted on May 20, 2002, including surrogate recovery data.

NYC-WTC_000024319–000024332

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024328
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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\020509\10208.D Vial: 10 Acq On 9 May 2002 7:31 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Morpholine, 4-[3-(4-butoxyp. .. Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.83 0.50 ug/1 78785 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Morpholine, 4-[3-(4-butoxyphenox... 293 C17H27NO3 000140-65-8 72 2 Furaltadone 324 C13H16N4O6 000139-91-3 72 3 N-Morpholinomethyl-isopropyl-sul... 175 C8H17NOS 1000145-15-9 45 4 Morpholine, 4-[3-(4-butoxyphenox... 293 C17H27NO3 000140-65-8 40 Abundance Scan 5234 (33.832 min): 10208.D (-5223) (-) m/z 100.10 100.00% 100

5000 . sr J T-1 r . f ! ,

33.40 33.60 33.80 34.00 34.20 1 55 70 84 ' ' I1")'. .-'tH r'7' ri'.. 126 255 m/z 41.20 7.89% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #118669: Morpholine, 4-[3-(4-butoxyphenoxy)propyl]- 100 128

5000 4... Mu Pnh . / In 33.40 33.60 33.80 34.00 34.20 m/ z 43.10 6.35% 41 , 56 70 86 113 293 ■ ■ ।1 Tr "ii 11* 150 166 ■ ■ i'1 ■' i 1 ■1 ■ i ■' 205 236 ■ i ■' ■ ■ i ■ ■ ■' i ■' ■ ■ i ■ ■ ■11 ■ ■ ■ ■ । iz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #118637: Furaltadone 100 hl , AA M AAMA 1 luqudhu 33.40 33.60 33.80 34.00 34.20 5000 m/z 42.10 6.00%

42 56 70 .128.. 185..... ■■i1 mongus mz->_____ 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #43577: N-Morpholinomethyl-isopropyl-sulfide A A , , AAA A i ' ■ 1 • । * 1 * 1 f • 11 ' । 100 33.40 33.60 33.80 34.00 34.20 m/z 55.10 5.66% 5000

43 56 ., ii, T 70.., 1 1 | I I I11 I I' I • I ! 1 AMAA .44 I 111 1 1 ' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 33.40 33.60 33.80 34.00 34.20

10208.D SCAN020507.M Tue May 14 14:22:36 2002 Page 6

NYC-WTC_000024328

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NYC-WTC_000024328Source: NYC Law Department, mirrored locally

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