GCMS quantitation results for sample AE10241, May 2002

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Laboratory report documenting GCMS analysis of sample AE10241 conducted on May 28, 2002.

NYC-WTC_000024780–000024790

Folder label: “GCMS X 5/14/02 A 5/17/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10241 ,D Vial: 19 Acq On : 10 May 2002 4:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Morpholine, 4-octadecyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 38.60 0.67 ug/1 73363 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Morpholine, 4-octadecyl- 339 C22H45NO 016528-77-1 64 2 1-Propanol, 2-methyl-2-(propylam... 235 C14H21NO2 000495-70-5 56 3 4,9-Decadien-2-amine, N-butyl- 209 C14H27N 062238-25-9 50 4 Furaltadone 324 C13H16N406 000139-91-3 50 Abundance Scan 6045 (38.597 min): 10241 .D (-6035) (-) m/z 100.10 100.00% 100

5000

i11111 ■ ।1111 — r11ni ।11 43 38.20 38.40 38.60 38.80 39.00 y —++7985. TOT126 144 220 310 —Tumpuun———u—mm—TmOOT—TT m/ z 43.20 6.76% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43779: Morpholine, 4-octadecyl- 100

5000 mMvMMVYPWrhN 38.20 38.40 38.60 38.80 39.00 m/z 42.10 5.80%

n/z-> 20 ,2743+79.85, 40 60 126141156 184 212 232 252268 294310 ' ■ i " ■ ■ i ■ " ' i ■ " ' i' " ‘ i1 ■1 ■ i ■ " 11 ■ ■111111' 111" I' " 11111 ‘I " 80 100 120 140 160 180 200 220 240 260 280 300 320 340 338

Abundance #43787:1-Propanol, 2-methyl-2-(propylamino)-, benzoate 100

38.20 38.40 38.60 38.80 39.00 5000 m/ z 41.00 5.69%

58 77 41 177 — 118134 220236 " | | " I' " ' i " 1' 11'111" '' I " " I' " 11 " 111 " " [1 " I " m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43598:4,9-Decadien-2-amine, N-butyl- 100 38.20 38.40 38.60 38.80 39.00 m/z 101.00 5.23%

5000 44

/z—> + —A9—28 20 40 60 81 TItur 123138 166 194210 " i' ■ " i ■ " ■ i' " 11' ■ " r ■ ■ ........... ......................................... ITTI ।, 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■ ■ । 38.20 38.40 38.60 38.80 39.00 ■

10241.D SCAN020507.M Tue May 14 14:25:39 2002 Page 8

NYC-WTC_000024789

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