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GCMS analysis results for sample AE10207, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10207 conducted on May 17, 2002, including surrogate recovery data.

NYC-WTC_000024305–000024318

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024315
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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020509\10207.D Vial: 9 Acq On 9 May 2002 6:32 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\ni st 9 8.1

Peak Number 5 N-Nonanal N-methyl-N-formyl... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 36.51 0.41 ug/1 57947 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual l N-Nonanal N-methyl-N-formylhydra ... 198 C11H22N2O 061748-14-9 59 2 Morpholine, 4-octadecyl- 339 C22H45NO 016528-77-1 50 3 4-Morpholineethanamine 130 C6H14N20 002038-03-1 40 4 Butanamide, 2-(dimethylamino)-N-... 593 C35H39N5O4; 018397-13-2 39 Abundance Scan 5690 (36.511 min): 10207.D (-5682) (-) m/z 100.10 100.00% 100

5000

36.20 36.40 36.60 36.80

m/z-> 111149.5579.TTT 156 236 283 i' ■' ■i' ■ ■11 ■ ■■11 ■' 20 40 60 I80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■ i1 ■1 ‘ i' " ' i ■■ ■ ■ i111111 ■ ■ ■ i ■ ■ ■ • i " ''i m/z 101.20 6.99%

Abundance #43747: N-Nonanal N-methyl-N-formylhydrazone 41 85 100 59

5000 140 ...36.40I. ^, M36.20 l.. ... 36.60 36.80 m/z 55.10 6.46% 198 1 169 |_______________________ TTT TI TIi' ■1 ■ i ■ ■ ■ ■ i "1 ■ i'" ■ i ■'' ■ i ■1 ■ ■ i ■ ■ ■11 ■ •' ■ i"1 ■ i " n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340

AhliaukuznkknHmahh Abundance #43779: Morpholine, 4-octadecyl- 100 36.20 36.40 36.60 36.80 5000 m/z 43.20 5.05%

27 43 ,70 184 —212 232 —252268 nPmp ‘ 126141156 0B0—00—010""u ETmu21 294310 338 mOCOOOTTT /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #43637:4-Morpholineethanamine 100 36.20 36.40 36.60 36.80 m/z 41.05 4.53%

5000

56

n/z—> mh 30 130 111——-0100OT0*—uum—Tg 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Mpdahlanla.s.1 36,20 36,40 36,60 36.80

10207.D SCAN020507.M Tue May 14 14:22:18 2002 Page 7

NYC-WTC_000024315

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NYC-WTC_000024315Source: NYC Law Department, mirrored locally

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