GCMS analysis results for sample AE10207, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10207 conducted on May 17, 2002, including surrogate recovery data.

NYC-WTC_000024305–000024318

Folder label: “GCMS X 5/1/02 A 5/9/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020509\10207.D Vial: 9 Acq On 9 May 2002 6:32 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 6-Undecylamine Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 38.59 0.26 ug/1 35885 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6-Undecylamine 171 C11H25N 033788-00-0 36 2 6-Undecylamine 171 C11H25N 033788-00-0 36 3 1-Propanone, 2-(diethylamino)-1-... 205 C13H19NO 000090-84-6 9 4 Morpholine, 4-[3-(4-butoxyphenox... 293 C17H27NO3 000140-65-8 9 Abundance Scan 6044 (38,591 min): 10207.D (-6037) (-) m/z 100.10 100.00% 100

5000

■ I ‘ 1 I ‘ ‘ ' I LMM । । । । । । r । 43 57 70 86 38,20 38.40 38.60 38.80 39.00 11 11 i, | n n 11111 | , lllp 1111 u .'i | ′ 1111 ■ I 126 153 0 ■ "'11"' i"(l i‘ ■'' i1r'"' i"1 ‘1 I" "I"11111 "I" m/ Z 43.05 10.73% n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #43532:6-Undecylamine

5000, 30

43 55 100

Apou 38.20 38.40 38.60 38.80 39.00 m/z 57.10 5.86% 15 69 83 114 126 170 0 TTTWTTTTTTTTTT ‘01001 —0000—0771000050100110000—0— iz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210

AAAuLAaALMMMMuu Abundance #118625: 6-Undecylamine 100

38.20 38.40 38.60 38.80 39.00 5000 m/z 86.00 5.48% 30

1.3 556 83 o1'11 ■ ■ ■' । ■1'111 ■ ■ 1" " ।1 ′ । ■ ■ ■ ‘l ■" 'i , . 114 170 “ ।" ■■ ■ ■ ■ ■ ।11 ■ ■ ।" " । ■ ■ ■, । ■'1 ■ । ■ ■ ■ ■ I-, h ■ r1. ■ ■ ।1111111111111111' niz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #43718: 1-Propanone, 2-(diethylamino)-1-phenyl- 100 38.20 38.40 38.60 38.80 39.00 m/z 56.10 5.34%

5000

AA 72

nfz-> n 29 44 56 ,184 , I , 115 132 146 160 174 188 203 u " r "' i" " i" " i11" i'1111" " 111 ‘1P1" I'1"11" " 11111111111"'1111" 111111111' I"1' 11111111111'1 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 X 38.20 38.40 38.60 38.80 39.00

10207.D SCAN020507.M Fri May 17 15:48:47 2002 Page 1

NYC-WTC_000024316

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