GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) es Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 14 Undecane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.27 1.88 ug/1 135191 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Undecane 156 C11H24 001120-21-4 93 2 Hexadecane 226 C16H34 000544-76-3 86 3 Tetradecane 198 C14H30 000629-59-4 86 4 Undecane 156 C11H24 001120-21-4 81 Abundance Scan 1904 (14.266 min): 11284.D (-1897) (-) m/z 57.10 100.00% 43 57

5000 71 85 14.00 14.20 14.40 14.60

miz-> r...... 20 ../88 1 60 40 80 113/135 156 ................ 1 ‘i 1 ■ 1 ■ । 1 ■ • • j * • * < । * i* »।* * *।।i * < *।i» > * । * < » * । ■ * 100 120 140 160 180 200 220 m/z 43.05 90.90% Abundance #16533: Undecane 43 5 7

5000 71 14.00 14.20 14.40 14.60 85 29 m/z 41.10 50.60%

niz-> 15—14 20 40 i, , ,il, , . 4—r i" । rn i । 60 80 , 93 । 113 > 1,

100 127 156 ,,, i I j t । | । i t i i

120 140 160 180 t l i t

200 i i ।

220 । ~| 1

Abundance #112406: Hexadecane 43 57 71 14.00 14.20 14.40 14.60 5000 m/z 71.10 46.35% 85 29

1 sl404 60 [ .804.3 113,127 141.155 169.183. 226 niz-> 20 100 120 140 160 180 200 220 Abundance #112357: Tetradecane — P MM, +4 Mr 57 14.00 14.20 14.40 14.60 43 m/z 85.10 29.49% 71 5000 85 29 99 113 127 141 155 169 198 • ■ ।1 1 r" "T +—74 TT190 —u"mR—aameTT Ar 6444/ w A , Auapuah n/z—> 20 40 60 80 100 120 140 160 180 200 220 14.00 14.20 14.40 14.60

11284.D SCAN020507.M Fri May 17 13:06:43 2002 Page 17

NYC-WTC_000014799