GCMS analysis results for sample AE10703, May 20 2002

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Data File : C:\MSDCHEM\l\DATA\020513\10703.D Vial: 14 Acq On : 14 May 2002 1:24 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Hexatriacontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 30.17 0.29 ug/1 31798 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 59 2 1-Undecene, 4-methyl- 168 C12H24 074630-39-0 59 3 Tetratetracontane 619 C44H90 007098-22-8 59 4 Decane, 2,3,7-trimethyl- 184 C13H28 062238-13-5 59 Abundance ■ Scan 4610 (30.166 min): 10703.D (-4598) (-) m/z 57.10 100.00% 57

5000 85 A-A---A— J I).......................................................... ’I' , 126159 1 ' i 1 1 ' 1 i 1 1 1 ' i ■ 1 1 1 i ■ ■ ' 1 i ■ ■ ■ ■ i ■ ' 1 ' i 1 1 1 1 I 1 1 1 1 i' " । ' 1 1 । । 1 । 29.80 30 00 30 20 30.40 m/z 43.10 70.49% m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #112335: Hexatriacontane 57

5000 85 i #hpuAphouhul , ! MAkhohAuhnaah 29.80 30.00 30.20 30.40 m/z 71.05 64.75% ] 113141169197225 m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #5642: 1-Undecene, 4-methyl- 43

71 29.80 30.00 30.20 30.40 5000 m/ Z 85.20 39.55%

, 126 11 ; I 168 ...... . ....................... ............................ m/z~> I 100 150 200 250 300 350 400 450 500 550 600 Abundance 57 #112365: Tetratetracontane LAAALMALA 29.80 30.00 30.20 30.40 m/z 41.10 32.58% 5000 85

/z—> r I'T 50 100 113141169197225253281 309337365393 435463491519 561589617 f . > f J . 1

150 1 . '| f .-i )

200 250 | I . i i

300 | . . I I ■[ I

350 I I I

400 | I I I I

450 | I t"i I

500 | T I r I

550 I I I I I

600 | I | I Lhul 29.80 30.00 30.20 30.40

10703.D SCAN020507.M Wed May 15 08:59:07 2002 Page 6

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