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GCMS quantitation results for sample AE10243, May 2002

Machine-extracted title · confidence 90%

Laboratory report of GCMS analysis for sample AE10243 conducted on May 28, 2002.

NYC-WTC_000024813–000024823

Folder label: “GCMS X 5/14/02 A 5/17/02

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Scanned page image, NYC-WTC_000024822
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020516\10243.D Vial: 19 Acq On : 17 May 2002 3:08 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C : \DATABASE\nist98.1 ********************************************************************* Peak Number 4 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.33 ug/1 26427 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene -dlu 188 C14D10 001517-22-2 72 V2 Anthracene-diO- 188 C14D10 001719-06-8 53 3 13,5-Trimethyl-2-cyclopentylben... 188 C14H20 030628-31-0 9 4 Antipyrine 188 C11H12N2O 000060-80-0 9 Abundance Scan 4914 (31.952 min): 10243.D (-4907) (-) m/z 188.20 100.00% US

5000 80 94 160 66 106 134 31.60 31.80 32.00 32.20

m/z—> -RHH THTTTTTTTTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ''" i" " i1 rp-r 40.73% Abundance #79827: Phenanthrene-d10 188

5000 ' rl ' ' ' ' I ' 1 ' ‘ I ' 31,60 31.80 32.00 32.20 80 m/ z 94.2 0 22.60% 94 160 30 42 52 66 11 108118 132 146 ,|.| 170179 I" " i" " I" " 1........ . . . . . . 11111 rl 111 11—*———*— mfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d1 0 188

31.60 31.80 32.00 32.20 5000 m/z 160.10 19.04%

80 94 160 Ji 66

/z-> 17 30 42 52 TuunpuunmmupHur -HH +198118.132. 146—4179179 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79785:1,3,5-Trimethyl-2-cyclopentylbenzene 159 173 188 4 31.60 31.80 32.00 32.20 m/z 184.10 17.71%

5000 133 119 145

67 91 195 1. 1 ' i ’"11”' ■ i" " i' ■" i" " i ■"' i" " i ""i"' ‘ i ‘1" i" - J"" ' ' i 1 ' ‘ IT 1 rT1 ' < > । > 'ii । 1 m/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10243.D SCAN020507.M Fri May 17 10:43:10 2002 Page 6

NYC-WTC_000024822

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NYC-WTC_000024822Source: NYC Law Department, mirrored locally

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