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GCMS quantitation results for sample AE10247, May 2002

Machine-extracted title · confidence 90%

Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.

NYC-WTC_000024896–000024906

Folder label: “GCMS X 5/14/02 A 5/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020516\10247 -D Vial: 23 Acq On : 17 May 2002 7:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 1,4-Naphthalenedione, 2-hyd... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.27 ug/1 22173 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual e, 2-hydroxy-... 188 C11H803 000483-55-6 37 2 Anthracene-dlO- 188 C14D10 001719-06-8 36 3 Phenanthrene-d10 188 C14D10 001517-22-2 36 4.Ant ipyr ine 188 C11H12N2O 000060-80-0 32 Abundance Scan 4914 (31.952 min): 10247.D (-4907) (-) m/z 188.15 100.00% 1(18

5000 94

160

n/z-> . 49 ■ ।• • ■ ■।■1 ■ ।111 >11■ i • •" । 80 ,। 11> i >'■ ■ 11 s 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 1’1" 31,60 31.80 32.00 32.20 m/z94.10 41.54%

Abundance #125707:1,4-Naphthalenedione, 2-hydroxy-3-methyl- 158

5000 ■ ■ i ■ • ' TTT tmr । । । । । । , , , । , 31.60 31.80 32.00 32.20 m/z 184.10 31.68% 50 77 105 131 160 m/z-> 11" " ।1 ■" । । " I'"'' ..... ......... 1,115... 1........ 1....... r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 ""I 31.60 31.80 32.00 32.20 5000 m/ Z 189.30 24.42%

66 80 94 160 , , 17 30 42 52 । , , 108118 132 146 ,|| 170179.1 TTTTTTTTTTTTTTTTTTH 11'1111" H r" " 111" i11111" " i1" 'i ।1' 11 >11111' "l’l’ 11111111 FMri., m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 31.60 31.80 32.00 32.20 m/ z 160.20 18.16%

5000

80 94 160 30 42 52 68 , ,1 108118 132 146 ,|. 170179.1,1 | TDTTTTTTTTTTTTHTTHH —uu—tTHTIITTTTTTT m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10247.D SCAN020507.M Fri May 17 10:49:54 2002 Page 6

NYC-WTC_000024905

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NYC-WTC_000024905Source: NYC Law Department, mirrored locally

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