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GCMS sample analysis results for unknowns, May 2002

Machine-extracted title · confidence 95%

Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10130 on May 17, 2002.

NYC-WTC_000046159–000046169

Folder label: “GCMS X 5/7/02 A 5/14/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10130.D Vial: 17 Acq On : 14 May 2002 4:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title Method 508 GC/MS Scan Library C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.35 ug/1 37563 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Anthracene-dl0- 188 C14D10 001719-06-8 80 2 Phenanthrene-d10 188 C14D10 001517-22-2 72 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 53 4 Naphthalene, 1,5-dimethoxy-_________ 188 C12H1202 010075-63-5 53 Abundance I Scan 4915 (31.958 min): 10130.D (-4908) (-) m/z 188.20 100.00% / 188

5000

, y.................. 80 158 । 31.60 31.80 32.00 32.20 54 I I no 356 --HA TIOWWPTTIPug 1-q-T m/z 184.10 15.17% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #79826: Anthracene-d10- 188

5000 IIIIIII11II 31.60 31.80 32.00 32.20 m/z 189.20 14.17% — 94 160

■n/z-> 17.42.6644114132 —4 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 111111111111111110111101"7‘0T101T"TTTE"TTTTT

Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/z 80.30 13.55%

80 160

•n/z-> 30 1 " i ■11' I'1 20 40 5260— 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 .i 100 I 32 l T Iirl’i i I i | i | I I | i r rf < i

Abundance #79804: Naphthalene, 1,7-dimethoxy- 188 31.60 31.80 32.00 32.20 m/z 78.10 13.11%

5000 115 145

63 !94 TTIWITITTTTTTTT II ' I'' ", I'11 '11'''11'11111 ‘ I‘‘‘‘N‘‘‘‘A‘‘AA‘A‘‘A‘‘A‘dA‘A/I‘+**}*I/5 TT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 31.60 31.80 32.00 32.20

10130 .D SCAN020507.M Tue May 14 15:58:29 2002 Page 6

NYC-WTC_000046168

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NYC-WTC_000046168Source: NYC Law Department, mirrored locally

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