GCMS analysis results for sample AE11158, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020515\11158.D Vial: 10 Acq On : 15 May 2002 8:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.39 ug/1 38240 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 64 2 P enanthrene - dl 0 188 C14D10 001517-22-2 64 3 2 2,9, 9-Tetramethyldec-5-ene-3,7 . . . 188 C14H20 102745-35-7 37 4 A .tipyrine 188 C11H12N2O 000060-80-0 28 Abundal Scan 4914 (31.952 min): 11158.D (-4904) (-) m/z 188.20 100.00% 188

5000 94

80 44 64 158 . 31.60 31.80 32.00 32.20 ----- - i ■1" i m/z 94.00 37.47% /z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-dlO- 188

5000 _ ...................... ■ ' I ' I ■ ' | ' 1 Fd r I I I IT I I | I 31.60 31.80 32.00 32.20 m/z 189.00 18.80% ee 80 94 160 , 17 30 42 52 ° . , 108118 132 146 ,1 170179 11 niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 .......... ...............................

31.60 31.80 32.00 32.20 5000 m/z 80.00 16.36%

80 94 160 30 42 52 66 . 11 108 118 132 146 II 170179|,| TTWTTTTTTTTTTTHTTTTHTTTTgT "T mlz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79801:2,2,9,9-Tetramethyldec-5-ene-3,7-diyne 158 31.60 31.80 32.00 32.20 173 m/z 184.10 13.23% 41 131 143 91 5000 77 158 57 119 27 67 105

/z—> ■1'I''1111 #H#lHHAl#H4.#+p + u 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160170 180 190 W 31.60 31.80 32.00 32.20

11158.D SCAN020507.M Thu May 16 09:53:07 2002 Page 6

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