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GCMS analysis results for sample AE11280, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11280 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024730–000024742

Folder label: “GCMS X 5/13/02 A 5/15/02

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Scanned page image, NYC-WTC_000024740
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NYC 9/11 Public Portal Document Library search compound Report Data File : C:\MSDCHEM\l\DATA\020515\11280.D Vial: 14 Acq On : 16 May 2002 12:39 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.32 ug/1 35523 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

V 1 Anthracene-dlO- 188 C14D10 001719-06-8 93 2 Phenanthrene-d10 188 C14D10 001517-22-2 90 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) ... 188 C14H20 1000215-61-8 40 4 _ (4- Tolyl) -3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 37 Abundance Scan 4913 (31.946 min): 11280.D (-4906) (-) m/z 188.20 100.00% 188

5000 94 AO 66 158 31.60 31.80 32.00 32.20 344 n/z-> ..... 4211. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 " i " " i ■ " ' 111'11r" ' i " " i111111" m/ z 94.00 25.47% Abundance #79826: Anthracene-d10- 188 ............ (........................................ 5000 31.60 31.80 32.00 32.20 m/z 189.10 18.41% 94 17 42 66 i „ il 114 132 TI’T Tmtt ' i " " r ■' ■ i " " i " " i " " i " " i'' nz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79827: Phenanthrene-d10 188 31.60 31.80 32.00 32.20 5000 m/z 184.10 16.22%

80 160

mz-> T’li 30 11'1 52,1 . 4. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 11 ■1" i ■ " ' i ■" ■ i" " i'" ■ i1'" i''

Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11)tetradeca... 188 31,60 31.80 32.00 32.20 m/ z .80.10 15.29% 5000 91 55 131

-n/z-> " I'1 20 .4,8.4.4/2874-HH# 159 " i " " i" “ i " " i ■ " ' i1" 11"11111" i " ! I | f l , PP I ‘f I [ ‘ I I I I |' I

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31,60 31,80 32.00 32.20

11280.D SCAN020507.M Thu May 16 09:59:23 2002 Page 7

NYC-WTC_000024740

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NYC-WTC_000024740Source: NYC Law Department, mirrored locally

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