GCMS analysis results for sample AE11303, May 2002

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Laboratory report documenting GCMS analysis of sample AE11303 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024585–000024595

Folder label: “GCMS X 5/13/02 A 5/16/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020516\11303.D vial: 14 Acq On : 16 May 2002 10:12 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.31 ug/1 23708 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

< 1 Anthracene-dlO- 188 C14D10 001719-06-8 72 2 Phenanthrene -diO 188 C14D10 001517-22-2 50 3 Pyntacyclo[8.4.0.0(3,7) .0(4,14) . . . . 188 C14H20 1000099-27-2 9 4 4H-Pyrido[1,2-a]pyrimidin-4-one,... 188 C11H12N2O 057773-19-0 9 Abundance Scan 4915 (31.958 min): 11303.D (-4904) (-) m/z 188.20 100.00% 188

5000

94 66 80 158 170 31.60 31.80 32.00 32.20

n/z-> ............ . ..... l.sI.. + 1' 11'1' 11''11''1111 polaagm ITT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 189.10 26.18% Abundance #79826: Anthracene-d1 fl- 188

------- 5000 31.60 31.80 32.00 32.20 m/ z .94.20 19.59% 80 94 160 | 17 30 42 52 ° , J 108118 132 146 I 170179 TETOTTHTHTHtTTt TTTur /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 , I f , ri , , I ri . , , , | . I . . J . 31.60 31.80 32.00 32.20 5000 m/z 184.00 18.31%

80 94 160 30 42 52 66 11 108 118 132 146 ,|,| 170179.1,1 T—mTmWTRTTTTTTHTTHTTTTTTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79714: Pentacycto[8.4.0.0(3,7).0(4,14).0(6,11)]tetradecane 188 31,60 31.80 32.00 32.20 m/z 80.10 13.14% 5000 79 91 106 117 131 145 159 173

■n/z-> 27 41 — 00 11" " i" ’’’’i ■ ■ 67 ] 1-llpll44 1.. PAr.... L 11I—u—0—COOOTOTT" fr-rrT- 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 . । r . , । , ,-r । । > । । । । । । , । । 31.60 31.80 32.00 32.20

11303.D SCAN020507.M Fri May 17 13:09:48 2002 Page 6

NYC-WTC_000024594

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