GCMS analysis results for sample AE11303, May 2002

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Laboratory report documenting GCMS analysis of sample AE11303 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024585–000024595

Folder label: “GCMS X 5/13/02 A 5/16/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020516\11303.D Vial: 14 Acq On : 16 May 2002 10:12 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene, tetradecahydro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

31.08 0.22 ug/1 16677 Phenanthrene- dl 0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene, tetradecahydro- 192 C14H24 006596-35-6 53 2 Anthracene, tetradecahydro-, (4a... 192 C14H24 001755-19-7 50 3 2,4-Diamino-6- (hydroxymethyl) pte.. . 192 C7H8N6O 000945-24-4 33 4 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 28 Abundance 7 Scan 4766 (31.082 min): 11303.D (-4760) (-) m/z 192.10 100.00% 192

5000

96 146 ‘ I’’ 4....... 30.80 31.00 31.20 31.40 49 66 86108 _______ | _____________ " i'1" 11 r" i1" 'T11ITF 11111' 111 > । I 11L111—hpOTTTTTT "1111 m/z 146.10 20.17% niz-> 20 30 40 50 60 70 . 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80931: Anthracene, tetradecahydro- 135 192

67 81 95 । — । । । । । Uh 5000 41 121 I 1 1 1 1 I 1 1 55 150 30.80 31.00 31.20 31.40 110 m/ Z 96.30 19.70%

miz-? 29 sHmsipreer " I "1 r Tt L 163177 1 ''i *' । । ■ 11'. । । ■ i'i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L Abundance #80932: Anthracene, tetradecahydro-, (4a.alpha.,8a.alpha.... 192 135 30.80 31.00 31.20 31.40 67 m/z 193.20 15.45% 5000 81 95 55 121 150

m/z-> L -TT 163 177 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 " ' I''

Abundance #125821:2,4-Diamino-6-(hydroxymethyl)pteridine 43 192 30.80 31.00 31.20 31.40 163 m/z 194.10 13.91% 5000 28 53 68 146 175

n/z-> -H 92 111 77 ----- 106 121 133

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ll TI 30.80 31.00 31.20 31.40

11303.D SCAN020507.M Fri May 17 13:09:46 2002 Page 5

NYC-WTC_000024593

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