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GCMS results for sample AE11566, May 29, 2002

Machine-extracted title · confidence 100%

Laboratory report of GCMS analysis for sample AE11566 conducted on May 29, 2002.

NYC-WTC_000022598–000022608

Folder label: “GCMS X 5/17/12 A 5/21/02

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Scanned page image, NYC-WTC_000022606
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020521\11566.D Vial: 17 Acq On : 22 May 2002 12:10 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Anthracene, tetradecahydro-... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.31 ug/1 32711 Phenanthrene- dl 0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, tetradecahydro-, (4a... 192 C14H24 001755-19-7 53 2 Anthracene, tetradecahydro- 192 C14H24 006596-35-6 50 3 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 47 4 2,4-Diyamino-6-(hydroxymethyl) pte .. . 192 C7H8N60 000945-24-4 47 Abundance Scan 4767 (31.088 min): 11566.D (-4757) (-) m/z 192.20 100.00% 19 2

5000 96 ■ • i > ■ 49 66 82 118 146 160 || ' ■ I 1 1

iz-> 0 +40,444444 ----- 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 30.80 31.00 31.20 31.40 96.10 26.65% Abundance #80932: Anthracene, tetradecahydro-, (4a.alpha.,8a.alpha.„„ 192 135

5000 67 81 95 MMl. 30.80 31.00 31.20 31.40 55 121 150

MerMAMMHMguweA m/z 49.10 16.67% , , 110

m/z- > 0- L.. ................... ... It.. j.. L.Xi x.... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80931: Anthracene, tetradecahydro- 135 1912

67 30.80 31,00 31.20 31.40 81 95 5000 41 121 m/z 193.00 14.81% 55 150 110 29 0-TITt' 11 Ii ■ । prr r —pmot T L 13 177 miz-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80958:2,4-Diamino-6-(hydroxymethyl)pteridine 192 ..... HJ..... 43 163 30,80 31.00 31.20 31.40 m/ z 82.00 14.59% 5000 28 53 68 . 146 176 , 77 92 106 121 133

m/z-> 0 -Hll++ rll. । .'i । r lire । vr .., ....... . । 4tlL, — 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 T’l" 30.80 31.00 31.20 31.40

11566.D SCAN020521.M Fri May 24 09:40:07 2002 Page 5

NYC-WTC_000022606

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NYC-WTC_000022606Source: NYC Law Department, mirrored locally

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