GCMS analysis results, sample AE10701, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020513\10701.D Vial: 12 Acq On : 13 May 2002 11:24 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.35 ug/1 35188 Phenanthrene-dl0 31: 72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 87 2 Pentacyclo[7. 3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 64 3 Phenanthrene-diO 188 C14D10 001517-22-2 64 4 Phosphonic acid, (3-methyl-3-pen... 188 C8H13O3P 022152-34-7 58 Abundance / Scan 4915 (31.958 min): 10701 .D (-4905) (-) m/z 188.10 100.00% 188

5000

AS 80 94 160 । 31.60 31.80 32.00 32.20

m/z-> 41 52 I I ll 11 " " I " " I " " I...... I " 1 'T' " > |111 ’ /1 " 111' > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132 , |, 171 1111 ‘' i " " i'" r " ' 111 ’11"111" " i''' I ,J m/z 187.20 16.52% Abundance #79826: Anthracene-d10- 188

)............................... 5000 1 i ■ 1 1 1 1 ' ■ ■ 1 I ■ 1 1 1 i ■ ■ 1 ■ i ■ 31.60 31.80 32.00 32.20 m/z 80.20 15.17% 66 80 94 160 , . 17 30 42 52 ! . J 108 118 132 146 I. 170179 TIWWTTIPWWTIWTTIWUHHTT | t I I i , i i I I | । t 1 | I I । । 11 ri I ] I M 1 । 1 I i i |l i t r | I । t । | । 1 iTp i ri TTTITTTTrr /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11)]tetradeca... 188 - 31.60 31.80 32.00 32.20 5000 79 91 m/z 93.90 14.20% 55 67 105 131 100 117 m/z-> 11" " i " " i ■1 ‘11' 1 all U ++— 145 152173.. 11... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 • I 1 ′′′ | .... | i | | . T| ′′′′

Abundance #79827: Phenanthrene-d10 188 31.60 31.80 32.00 32.20 m/z 160.10 11.39%

5000

80 94 160 30 42 52 66 1WPnnun)——umHr 11 108 118 132 146 I’1 ri I1"11 ■■1' i ■" ■ 1111 ■ i1" 11 +44,1179179444—. m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10701 .D SCAN020507.M Wed May 15 08:41:59 2002 Page 7

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