GCMS analysis results, sample AE10135, May 2002

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Data File : C:\MSDCHEM\1\DATA\020513\10135.D Vial: 21 Acq On : 14 May 2002 8:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.33 ug/1 35629 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 58 2 Phenanthrene-diO 188 C14D10 001517-22-2 58 3 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 32 4 4M-Pyrido[1,2-a]pyrimidin-4-one,... 188 C11H12N2O 057773-19-0 32 Abundance Scan 4913 (31.946 min): 10135.D (-4907) (-) m/z 188.20 100.00% / 188

5000 80 47 RA <34 156 326 31.60 31.80 32.00 32.20 rrrl / I1! 1 I, 1,77 /z-> ’ ’I’ Mk... I t l l < < > I I I I I I ( I I I I I I I I [ I I

20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 I' 1' m/z .80.10 27.19% Abundance #79826: Anthracene-d10- 108

5000 TT l ■ ■ ■ ■ । । । 1 । > • । । 31.60 31.80 32.00 32.20 m/ z 184.20 25.95% 94 160

m/z-> 17,11142 .. . A1141324 I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 TT" i'1' ‘ ।111 ■ i ■' ■ ■ i ■ ■ ■ ■ i ■'

Abundance #79827: Phenanthrene-d10 188 I’IYMIIIFIIIIIIIIIIII 31.60 31.80 32.00 32.20 5000 m/z 94.10 24.96%

80 160 II 30 I .1 52111 , I 1, | I II | 1T [' I — i 100 132 1 ri i । mnfm ■ ’ i ■ ■1 ■ ।1 ■11111 *111111 r 1111 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 31.60 31.80 32.00 32.20 m/z 189.20 16.44% 5000

143 89 115 . 170 64 "I'-......... 11") __i.I 1I >11I 11 ■ lir ■ । IT | I I I (’111 I ■ | I I I I | I I I I | i ■ ■ • ' । i 1 1 ■ । ’ 1 1 1 । r’ ■ ■ । /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 31.60 31.80 32.00 32.20

10135.D SCAN020507.M Wed May 15 08:30:29 2002 Page 6

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