GCMS analysis results for sample AE08427, May 2002

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Data File : C:\MSDCHEM\1\DATA\020419\08427.D Vial: 14 Acq On : 19 Apr 2002 8:56 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.36 ug/1 806229 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 91 2 Phenanthrene-dlO 188 C14D10 001517-22-2 86 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 42 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 4916 (31.963 min): 08427.D (-4903) (-) m/z 188.20 100.00% 188

5000 40

B0 94 TI 31.60 31.80 32.00 32.20 51 66..... | 136 146 160 .... ... ..... ■ i"111" " ।" 11 ....... rdetantt ■ ।'11 ■ । ■ ■ ■ ■ i ■ ■ " । " I " । ■ 11 ■ J11 > " 111 m/ z 4 0.10 42.99% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1(18

5000 31.60 31.80 32.00 32.20 m/z 94.10 17.88% 80 94 160 66 17 30 42 52 ' i " " i" " I" " 11"11111 +4198118,132,146—44170179—.. n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 TI I‘‘Ii i-i । । |—i-i । । । । 31.60 31.80 32.00 32.20 5000 m/z 80.10 15.72%

80 94 160 30 42 52 66 ' i"111'1" i1"11" " i1'111H'1111 'H1,1 'I ++108,118—132146—179179— n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 1(18 31.60 31.80 32.00 32.20 m/z 189.20 15.60% 5000

143 . 89 115

Tl/z-> n ‘1" ।1"11 51 64 76 . 102 I 130 11 ' I'1" i ‘ ' i' I’ i' ■ ‘I 'r'' i1 ■ ■ ■ i ■ I’ i111 r‘ 111 i'l '111 - 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 170 u Tf । 1 ■ ■ 11 1 1 1 1 i 1 • 1 1 i 1 31.60 31.80 32.00 32.20

08427.D SCAN020418.M Thu May 02 15:34:27 2002 Page 7

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