GCMS analysis results for sample AE08428, May 2002

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Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048195–000048206

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08428.D Vial: 15 Acq On : 19 Apr 2002 9:55 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.28 ug/1 641759 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 40 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 36 Abundance Scan 4915 (31.957 min): 08428.D (-4906) (-) m/z 188.10 100.00% 188

5000

40 80 94 158 | 52 66 31.60 31.80 32.00 32.20 TIWWPIWPTWPTTTTT i"' ■ i" " r " 11' I’T m/z 189.15 17.50% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1(18

5000 T 31.60 31.80 32.00 32.20 m/z94.10 17.21% 17 30 42 52 80 .94 160 i, 108118 132 146 |L| 170 179) I | I । । । | i ' > । | M i f | l i > > | I I i ( । I I I i । i । I | j | ( i I | TI 1 i | T I I I | I I I I | 1'1 rrrt 1 n | I I I I J I Pr‘ I I I | I I I I | I'l I | I | I ‘i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1(18 TI 31.60 31.80 32.00 32.20 5000 m/ z 80.10 13.32%

80 94 160 30 42 52 66 m/z-> rpri 111111111111111,111111111111111111 ii 11 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1 108 118 132 ThTTb 146—4170179 — TT

Abundance #79804: Naphthalene, 1,7-dimethoxy- 173 KB 31.60 31.80 32.00 32.20 m/z 184.10 13.12%

5000 102 115 145

m/z-> TTT 51 130 63 1 r " ' i " " 11 " 11' " ■ i ‘ " ■ r'" 11''''11' 158 "i1i' 75 l...... r'" i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m Til । 1 ■ 1 1 । 1 1 31.60 31.80 32.00 32.20 • i 1 1 1 1 i '

08428.D SCAN020418.M Thu May 02 15:36:07 2002 Page 6

NYC-WTC_000048204

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GCMS analysis results for sample AE08426, May 2002 · Box DEP Box 27

NYC-WTC_000048169

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

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