GCMS analysis results for sample AE08428, May 2002

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Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048195–000048206

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020419\08428.D Vial: 15 Acq On : 19 Apr 2002 9:55 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 31.10 0.29 ug/1 675994 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Bitoscanate 192 C8H4N2S2 004044-65-9 47 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 4 Phenanthrene, 3-methyl-_____________ 192 C15H12 000832-71-3 42 Abundance Scan 4768 (31.094 min): 08428.D (-4757) (-) m/z 192.05 100.00% 19 2

5000 40 ' ■ I ' ' 92 96 146 160 30.80 31.00 31.20 31.40 51 70| 82 | | 100 ' r " ■ i'1 1 ' ' ' Y' ' ' ' | | I I I I | ' H , | ! ! I I | I I > I | I I I I | I I I I rTMH | ■ I I I'l I I I I | I I I I | I I I 1 | Tprr m/ z 40.10 25.15% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 30.80 31.00 31.20 31.40 m/z 191.10 20.13%

mz-> . 96 29 39 51 63 74 83 t TTTT1T* l ' 11 rr l' 115 126 139 152 165 176 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 111 ■ ■

Abundance #125828: Bitoscanate 192 - 30.80 31.00 31.20 31.40 5000 m/z 193.10 15.67%

50 63 75 90 134 160 k I1?2, 122 148 176 ...... 4 ... lirfat) +++ Tp TT IHITm Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 ... yy... . 30.80 31.00 31.20 31.40 161 m/z 146.10 12.25%

5000 77 91 121 149 177 52 64 103

n/z-> ----- 1 "11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 '11" ■ „ . I. I " i ■ ■ 30.80 31.00 31.20 31.40

08428.D SCAN020418.M Thu May 02 15:36:05 2002 Page 5

NYC-WTC_000048203

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