GCMS analysis results for sample AE08063, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08063 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046740–000046756

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\DATA\020415\08063.D Vial : 20 Acq On : 16 Apr 2002 2:21 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C: \MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Phenanthrene, 9-methyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

22.64 0.22 ug/L 305045 Phenanthranene-dlO 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual J ( Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 40 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 36 Abundance Scan 3330 (22 645 min) 08063.D (-3322) (-) m/z 192.30 100.00% 15 2

5000 - 146 TT 82 96 2240 22.60 22 80 23.00 118 4 0 49 66 0 npm-tmmm 11'" ' i1 TT — m/z 191.30 23.16% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033 Phenanthrene, 9-methy- 192

5000 22.40 22 60 22.80 23.00 m/z 146.30 17.42% 96 165 i । 29 39 51 63 74 83 J 115 126 139 152 | 176 . 0- *IPBpUO———TgTTtTTPTTTTITTTTTNT"‘I /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953 2-Propenal, 3-(3,4-dimethoxyphenyl)- 15 2 161 22 40 22 60 22 80 23 00 5000 m/z 193.30 17.31% 77 121 149 177 91 . 103 52 64 138

/z-> 0 . > I < 11111. ■ rpi-. i r 11 > I. [‘k I >! T1! I >, >! J - r " 111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ... a Abundance #81034 Anthracene. 2-methyH 192 22.40 22.60 22 80 23.00 m/z 96.20 11.90% 5000 M 82 96 165

n/z-> 18 27 39 51 69 115 126 I | 1 39 1 52 1 0 11—aotpoddpuomhooB—uov"0d—Mhm I’I 1111| h 1 ,| n’i > 111 111 n’ 111 r" ।, । rl 1111111 it 1umn 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 | 176 11.. 11 22.40 22 60 22.80 23.00

08063.D 041202SCAN.M Tue Apr 16 13:51:59 2002 Page 11

NYC-WTC_000046754

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