GCMS analysis results for sample AE07976, April 18, 2002

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Laboratory report documenting GCMS analysis of sample AE07976 conducted on April 18, 2002.

NYC-WTC_000047593–000047607

Folder label: “GCMS X 4/4/02 A 4/15/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020415\07976.D Vial: 16 Acq On 15 Apr 2002 11:05 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Phenanthrene, 9-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.22 ug/L 267278 Phenanthranene- dl 0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 3 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 4 Anthracene, 9-methyl-________________ 192 C15H12 000779-02-2 40 Abundance Scan 3330 (22 645 min): 07976 D (-3322) (-) m/z 192.30 100.00% 152

5000

146 Igo ' ' I ' ' ' ' I ' ' 82 96 22.40 22 60 22.80 23.00 49 66 118 o. ।.... ।।. ।. PTT - P .................. ..... 117'' I m/z 191.30 19.30% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 I b 1 ' ■ I 2240 22.60 22.80 23.00 m/z 193.30 14.67% 29 39 51 63 75 83 0 ■।>■>■।■■■■।■■■•।•■■■। । ■ fl ■ ■ 11-- 115 126 139 152 96 | "If 165 1 176 i । J n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953. 2-Propenal, 3-(3,4-dimethoxypheny!)- 1912 161 2240 22.60 22.80 23.00 5000 m/z 146.30 14.20% 77 91 121 149 177 52 103

n/z-> Abundance 20 0 ■ । ■ ■ • ■ ।

30 >11 ■

40 l Hmm 50 60 70 64 .....| r ■ ■' i A .. ..... J,... 138

80 90 100 110 120 130 140 150 160 170 180 190 200 । ■■ ■■ I L #80950 1.5-Naphthalenedithiole I ■ ' ■ ■ l IB 192 22 40 22.60 22 80 23.00 m/z 96.20 11.01% 5000 1 115 128 159 } 40 57 69 79 147

/z- > 0 ----- 87,46,106,14— ' 44 —177. 136 | hfr 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 "TT i ■ • ■ ' i 22.40 22.60 22.80 23.00

07976.D 041202SCAN.M Tue Apr 16 13:46:09 2002 Page 9

NYC-WTC_000047605

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GCMS analysis results for sample AE07977, April 18, 2002 · Box DEP Box 27

NYC-WTC_000047608

Laboratory report documenting GCMS analysis of sample AE07977 conducted on April 18, 2002.

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