GCMS analysis results, Sample AE08265, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08265.D Vial: 22 Acq On : 18 Apr 2002 2:44 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Anthracene, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.32 ug/L 531602 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 3 2-Propenal, 3-(3,4-dimethoxyphen.. . 192 C11H1203 004497-40-9 42 4 Phenanthrene, 9-methyl-_____________ 192 C15H12 000883-20-5 40 Abundance Scan 3330 (22 645 min): 08265.0 (-3323) (-) m/z 192.10 100.00% 192

5000

8? 96 146 160 . /A.. 22.40 22 60 22 80 23 00 42 52 66 0 | 118 I I 0 TH Hp m/z 191.10 24.58% /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125847: Anthracene, 2-methyl- 192

5000 22 40 22.60 22.80 23 00 m/z 193.10 16.81% 28 39 51 63 74 82 96 115 126 139 152 165 176184 0- i rure rrr 111 i | 'i i < t | l,ri । 'I । fri |' l*i I’l i l'|*l | i i i । [* । ■ i ■ । । > ■ >'| । । । । 11 । । । । 1*1 • । । irrl > j i i i'l | I | ■ । । ■ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125845: Anthracene, 2-methyl- 192

2240 22.60 22.80 23.00 5000 m/z 146.10 14.62%

96 165 , 67 75 88 । 115 126 139 152 | 176 0- .... ....... hrHittftgasp. ।■ .-i.।. ‘| i n ।|'I,■ ■ ..... TT n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-( 3,4-di methoxy phenyl )- 1.2 22 40 22 60 22 80 23 00 161 m/z 160.10 12.28%

5000 77 121 149 177 91 103 52 64 138

Tl/Z--> 0 1... 1,— 20 30 40 p-rrrp- ’1111... I ’ ' I ' I I I I 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I'' ''I Hpr 22.40 22.60 22.80 23.00

08265.D 041702SCAN.M Thu Apr 18 09:58:19 2002 Page 15

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