GCMS analysis results, Sample AE08265, April 22, 2002

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GCMS analysis report for sample AE08265 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048378–000048400

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \MSDCHEM\1\DATA\020417\08265.D Vial: 22 Acq On : 18 Apr 2002 2:44 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.64 ug/L 1070920 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 94 2 Phenanthrene-dlO 188 C14D10 001517-22-2 90 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 36 Abundance Scan 3420 (23,174 min): 08265.D (-3414) (-) m/z 188.10 100.00% 188

5000

80 94 22.80 23.00 23.20 23.40 23.60 41 40 57 66 108 132 146 160 । I 0 i1 ■ " i ‘ ■ i1 -------■<‘i" ■11 ■"11 ■ ■■■ 11 "■ i > >" n 'milj...... 4pr m/z 189.10 15.63% n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-dIQ- 16 8

5000 t-|-i > ‘ ri FTH । । 22 80 23 00 23 20 23.40 23.60 m/z 94.05 15.61% 80 94 160 66 17 30 42 52 118 132 146 1 170 180 0 I " " 1111 ’I 1 > > 11 ■।111111 ptl TDTWIWTIH T n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 108 / 1 ’I 1 ' ' 1 1 ' T........... 22.80 23 00 23 20 23 40 23 60 5000 m/z 184.10 13.23%

80 94 160 30 42 52 66 n/z-> 10 0 , ’ 102110118 TT-1-r, p i i i j I i i 11 I | | । ! ■ I ]। "H I'M 11 !!■. 20 30 40 50 ■ I | | >r r 11 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132 146 1 'I1'"!.. ’l’ir 179.1894,.., n Abundance #79739: Cycloheptanone, 4-pheny- 18 8 22 80 23 00 23.20 23.40 23.60 117 104 m/ z 80.00 13.07% 91 160 5000 131 170

LI--+44 # 27 39 51 65 78 145 0 U 1’’ ‘ I’’ trmn Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23 40 23 60

08265.D 041702SCAN.M Thu Apr 18 09:58:19 2002 Page 16

NYC-WTC_000048397

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GCMS analysis results, Sample AE08266, April 22, 2002 · Box DEP Box 27

NYC-WTC_000048401

GCMS analysis report for sample AE08266 showing surrogate recovery and unknown compound screening on April 22, 2002.

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