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GCMS results sample AE08256, April 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08256 showing surrogate recovery and unknown compounds from April 2002.

NYC-WTC_000047886–000047903

Folder label: “GCMS X 4/8/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08256.D Vial: 14 Acq On : 17 Apr 2002 8:12 pm Operator: Nefliu Sample : sample Inst Instrumen Misc : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 23.18 0.63 ug/L 1073590 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 91 2 Phenanthrene-dlO 188 C14D10 001517-22-2 87 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 37 4 Pentacyclo[8.4.0.0(3,7) .0 (4,14) . . . . 188 C14H20 1000099-27-2 36 Abundance Scan 3420 (23 174 min): 08256.D (-3413) (-) m/z 188.10 100.00% 188

5000

94 43 57 71 80 112 132 146 188 170 1801 „ 22 80 23 00 23.20 23.40 23 60

n/z-> 0 1 10...... ......... mpilepaltundhe T‘ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TTt-j-rri f 111 11111 I 111 I f 11111 111111 11 [ m/z94.00 16.99% Abundance #79826: Anthracene-d10- 188

5000 22 80 23 00 23 20 23.40 23.60 m/z 189.10 16.44% RR 80 94 160 , 17 30 42 52 ° I 102 118 132 146 1 170 1801. 0 1 | । । " | 1 । 1 । | 1 I irtri I | । । ! I | । । I . | । I | . I . I | I I I । | I . । . | t I । . | I I . . | I I I ,| I . I I | । I I'l'l... . I I I I | l'l'll|l| I I I I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827 Phenanthrene-d10 108

22.80 23.00 23.20 23 40 23.60 5000 m/z 184.10 10.79%

80 94 160 | 30 42 52 66 II 102110118 .. 132 . | 146 . l . 170 189.., ... oV 111 ■ ■ | ■' | ■ | " " | H " !'' 1! t " It n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- ----- 108 TU 1 1 22 80 23 00 23.20 23.40 23 60 117 104 m/z 80.05 9.39% 91 160 5000 131 170 27 39 51 R5 78 145 । । 0I 00

n/Z- > 0 ........ . 1l. ' I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ll " i ■" . 1 'I 1 1 1 1 1 1 22 80 23 00 23.20 I-1 ‘ ‘IT 23.40 23.60

08256.D 041702SCAN.M Thu Apr 18 09:27:14 2002 Page 12

NYC-WTC_000047901

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NYC-WTC_000047901Source: NYC Law Department, mirrored locally

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