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GCMS results sample AE08256, April 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08256 showing surrogate recovery and unknown compounds from April 2002.

NYC-WTC_000047886–000047903

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047900
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08256.D Vial: 14 Acq On 17 Apr 2002 8:12 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 6 Phenanthrene, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.32 ug/L 541674 Phenanthranene-dl0 23.02

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 53 4 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 50 Abundance Scan 3330 (22 645 min): 08256.D (-3321) (-) m/z 192.10 100.00% 19 2

5000

R? 96 146 160 ........ *........ 1** 22.40 22.60 22 80 23 00 42 54 70 106 1187 .1 O' pmmmm—H .......... . 1............. pll TTr mj..... m/z 191.10 19.54% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842: Phenanthrene, 2-methyl- 102

5000 । ■ 1 1 ■ । ' 22 40 22 60 22 80 23.00 m/z 146.10 17.17% 96 27 39 51 63 74 82 | 115 126 139 152 165 176 . n/z-> ov ———T TTmvi.,,,... fl... । , ।, . ... ‘ I’’ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

2240 22 60 22.80 23 00 5000 m/z 193.10 15.40%

96 165 i । ft P +115,126,139/152476ll 29 39 51 63 75 83 n/z--> ov 20 30 40 50 60 70I 80 90 100 110 120 130 140 150 160 170 180 190 200 ■' i' ■

Abundance #125856: Phenanthrene, 1-methyl- — TT 19 2 2240 22 60 22 80 23 00 m/ z 96.00 13.47% 5000

96 1 115 126 139 152 A 100 178 . 27 39 51 63 74 82 n/Z-> ov **1'111. ..................... I " ’‘-I ■''' |‘*....... .... r+t rn4 " i" ■l 1 '"11. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 .......... 11............... i I 22.40 22.60 22.80 23.00

08256.D 041702SCAN.M Thu Apr 18 09:27:14 2002 Page 11

NYC-WTC_000047900

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NYC-WTC_000047900Source: NYC Law Department, mirrored locally

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