GCMS results sample AE08256, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08256.D Vial: 14 Acq On 17 Apr 2002 8:12 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Heptadecane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

21.82 0.24 ug/L 413208 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 93 2 Octacosane 394 C28H58 000630-02-4 80 3 Eicosane 282 C20H42 000112-95-8 78 4 Heptadecane___________________________ 240 C17H36 000629-78-7 74 Abundance Scan 3190 (21.822 min) 08256 D (-3183) (-) m/z 57.10 100.00% 57

5000 85 — Mr। । । *< । > , । rTm-mini । । r 21 40 :21 60 21.80 22 00 22.20 li 113 141 240 n/z- > 0- -mmmmmmmmmmmmmmmmmmmmmmmmmmmmPTT m/ z 71.10 65.74% 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #16420 Heptadecane 57

85 5000 f । । । / n * 21.40 :21.60 21.80 22 00 22 20 m/z 43.10 58.38%

UJ 29 0- I 113 1141 169 197 240 Ir‘l I fl i rr ine rr " i "on I ■ f rep | . r I. .. 11 .. I. f I 11 11 I ■ 11 |. 1. 11|. I. ] 11 11 11 > I 11 11 ! I 11 11 11 > 1 n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #112312 Octacosane 57 MAMPAANYAMAA/ , MMYAahn," Am 21.40 21.60 21.80 22.00 22 20 5000- m/ z 85.10 37.99% 85

29

n/z-> 0- 4 AA+ 141 169 li 113 —*TTUT—Tpuuum 197 225 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 253 281 309 337 365 394

Abundance #112343 Eicosane - 57 21.40 :21 60 21 80 22 00 22 20 m/ z 41.10 31.01%

5000 85 29

n/z—> 0 - j 113 141 169 pmm 282 ' i' " ’i " 11 r " 11 ” ■' i' ■'11 ■ ‘ " i " " p ogoov' 11 ■ - 'i' Mi , Asi / Yais 1 aAu 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 21 40 21 60 21 80 22.00 22 20

08256.D 041702SCAN.M Thu Apr 18 09:27:13 2002 Page 10

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