GCMS sample analysis results for AE10606, May 10 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10606.D Vial: 11 Acq On 7 May 2002 9:17 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Hexadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

21.76 0.23 ug/L 265349 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3/83 2 Eicosane 282 C20H42 000112-95-8 83 3 Heptadecane 240 C17H36 000629-78-7 78 4 Hexadecane 226 C16H34 000544-76-3 72 Abundance Scan 3179 (21.758 min): 10606.D (-3169) (-) m/z 57.10 100.00% 57 43 71

5000 85

A 99 , | 113 21.40 21.60 21.80 22.00 1 i 1 1 ■ 1 1 ' rl ' 1 , ! l|l, , , I , , |I. ..... a........... m/ z 43.10 73.16% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #112408: Hexadecane 43 57

5000 71 NAAAAA N Wi A a r mA A 1 1 111 1 i ■ 1 ■ ■ । 1 ■ ■ 1 । ■ ■ r ■ । ■ 21.40 21.60 21.80 22.00 85 m/z 71.10 29 68.55% „ 99 113127141 155169183197 — ,' 1 i 226 ' I 1 1 ' 'T ■ ■ i **11’a1***I*’**’*II**’I’**II’I* /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #109630: Eicosane 43 517 ......... A............ 71 21.40 21.60 21.80 22.00 5000 m/z 85.10 48.58% 85

99

n/z-s 20 40 ll 60 h j 113127141 155169183197 211 225239 253 267 282 80 100 120 140 160 180 200 220 240 260 280 Abundance #112319: Heptadecane ' i 1 ' ' ' i ' 57 21.40 21.60 21.80 22.00 43 m/ z 41.10 35.10% 71 5000 85 29

m/z-> 20 4. 40 n 99 113 127 141 155 169 183 —TTT—du—0Tmumun’,—TTuTT 240 60 80 100 120 140 160 180 200 220 240 260 280 .... Lu J. J....... 4 1 I ' 1 ' 1 1 11 1 1 T-—003"U/1 < 1 1 | v 21.40 21.60 21.80 22.00

10606.D 050102.M Thu May 09 09:12:04 2002 Page 9

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