GCMS calculation results for sample AE11602, May 2002

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GCMS analysis report for sample AE11602 dated June 4, 2002, documenting unknown compounds and surrogate recovery.

NYC-WTC_000013921–000013942

Folder label: “GCMS X 5/24/02 A 5/28/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052802\11602.D Vial: 8 Acq On : 28 May 2002 8:00 pm Operator: McLean Sample : 5/24 ad re-ext Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan *= Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Anthracene-dlO- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.31 ug/L 312326 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 80 ) 2 Phenant hrene-d10 188 C14D10 001517-22-2 37 3 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 33 4 1,4-Naphthalenedione, 2-hydroxy-... 188 C11H8O3 000483-55-6 28 Abundance Scan 3401 (23.062 min): 11602.D (-3395) (-) m/z 188.10 100.00% 188

5000 ......................................... 80 94 160 22.80 23,00 23.20 23.40

nfe-> 0 49 66 mmmmmpmmmmm m 10 20 30 40 50 60 70 80 90 100110120130140150 160170180190 I’t m/z 189.10 20.35% Abundance #79826: Anthracene-d10- 158

5000' 22.80 23.00 23.20 23.40 m/z 94.10 19.87% kr 80 94 160 , , 17 30 42 52 ° J , 108118. 132 146 11 170179 ,, 0-TIWTTTIWTTWTNTWTTHTTNTTHTtt niz—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 1 22.80 23.00 23.20 23.40 5000 m/z 184.10 14.33%

80 94 160 30 42 52 66 , 11 [I1Frrtt108118 0 11—20110011117 istsssp—sspoogardtveti 132 146 ,|. 170179,1,1 | up r 1 i I h 1111II11II1111 "’t’t" I TImmn n/z-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79714: Pentacyclo[8.4.0.0(3l7).0(4,14).0(6,11)]tetradecane - 188 22.80 23.00 23.20 23.40 m/z 80.10 14.22 5000 79 91 , .. 106 117 131 145 159 173

■nfe-> 27.55 ll— lHH++L.p. 0 ‘TE101mTETTTT 1‘1nr 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 ■ ■ I • • ' nj ’ ru । i i > > । । ■ 22.80 23.00 23.20 23.40

11602.D 052202.M Thu May 30 10:38:12 2002 Page 16

NYC-WTC_000013941

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NYC-WTC_000013941Source: NYC Law Department, mirrored locally

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