GCMS analysis results for sample AE11928, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11928.D Vial: 8 Acq On : 23 May 2002 3:40 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Anthracene-dlO- Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.28 ug/L 316999 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Anthracene-dlO- 188 C14D10 001719-06-8 94 2 Phenanthrene-diO 188 C14D10 001517-22-2 91 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 Abundance Scan 3402 (23.068 min): 11928.D (-3395) (-) m/z 188.15 100.00% US

5000

80 94 54 66 160 L 22.80 23.00 23.20 23.40 0-mmppmpmmpe ----- i * •' • i m/z 94.00 17.05% n/z-> 10 2030405060 70 8090 100110120130140150 160170180190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 16.08% ee 80 94 160 , , 17 30 42 52 66 „ 108118 132 146 ,|I 170179 0-mPWmpTHntptt Tt‘I n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188 ■ ■ ■ ■ । ■1 • * i ’* ।।. 22.80 23.00 23.20 23.40 5000 m/z 184.10 15.44%

94 80 160 30 42 52 66 iz-> 0 ,l | 'Tp-rrTp-rrrI-rTTTTtT^ mm 108118 132 146 11, 170179,1,1 10 2030405060 70 8090 100110120130140150 160170180190 ‘I Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/z 80.10 11.59% 145 5000

63 77 89 102 117 130 , 159 173 , m/z—> O-TPT*+- 41 51 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 I. -- 22.80 23.00 23.20 23.40

11928.D 052202.M Wed May 29 09:48:52 2002 Page 16

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