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GCMS analysis results for sample AE12162, June 2002

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Laboratory report documenting GCMS analysis of sample AE12162 conducted on June 5, 2002.

NYC-WTC_000013643–000013665

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise . Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Anthracene-dlO- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.25 ug/L 227936 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 80 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 Abundance Scan 3402 (23.068 min): 12162.D (-3396) (-) m/z 188.10 100.00% 188

5000

80 94 158 22.80 23.00 23.20 23.40 0- ---p--p--#-#9,-49,---—-+-p-+-+-++---H-F++F+7 m/z 94.10 19.51% niz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 17.95% . 80 94 160 , , 17 30 42 52 66 , J 108118 132 146 II 170179 0 109—** m/z-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 80.10 16.92%

80 Q4 160 30 i r|42 II li [ rl66 11 11 |52 I ■ 1111'l 111111111 108118 132 146 II 1701791 0-TWWTINIIT —mHHHTtun miz-> 10 2030405060 70 8090 100110120 130140150 160170180190 — Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 118 22.80 23.00 23.20 23.40 m/z 184.10 14.66%

5000 143

0- 64 76 88 102 115 130 ----- + mpmmmm-HH-m 51 1 158 170 n/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12162.D 052202.M Wed May 29 09:55:13 2002 Page 14

NYC-WTC_000013661

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NYC-WTC_000013661Source: NYC Law Department, mirrored locally

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