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GCMS analysis results, sample AE12531, June 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE12531 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014509–000014531

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\ 1 \DATA\05290212531.D Vial: 22 Acq On : 30 May 2002 3:11 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Anthracene-dlO- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 23.07 0.34 ug/L 392408 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 93 2 Phenanthrene-diO 188 C14D10 001517-22-2 83 3 2-Quinolinecarboxaldehyde, 8-hyd. .. 188 C10H8N2O2 005603-22-5 42 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3402 (23.068 min): 12531 .D (-3396) (-) m/z 188.10 100.00% 188

5000

80 94 160 22.80 23.00 23.20 23.40 40 .I 57 66 , 0 mmmmmmpmm— ■ i “ •' i “ “ i “ “ i “ “ i 11’4’11’ 1"11 m/z 94.00 15.60% /z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 184.10 14.85% 80 94 160 , . 17 30 42 52 0- 'I'"‘I ""I" THmHtt 66 , 108118 132 146 ,|.I 170179.1 TIHmm miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 118

22.80 23.00 23.20 23.40 5000 m/z 7.9.95 14.58%

94 80 160 30 42 52 66 11 .108118 132 146 11,| 170179,1 0 1PWIPIPPTTTHTTTH TTNTTTTNTTTTTTT n/z-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 22.80 23.00 23.20 23.40 m/z 189.10 13.93%

5000

64 76 89 1 102 115I. 130 W 158 170 . 0-mm 51 -HHl— TTTTTTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12531.D 052202.M Mon Jun 03 11:43:18 2002 Page 17

NYC-WTC_000014530

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NYC-WTC_000014530Source: NYC Law Department, mirrored locally

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