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GCMS sample AE11576 results, June 6 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis report for sample AE11576 detecting unknown compounds and surrogates on June 6, 2002.

NYC-WTC_000015561–000015580

Folder label: “GCMS X 6/4/02 A 6/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\060402\11576.D Vial: 9 Acq On 4 Jun 2002 10:22 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Anthracene-d10- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.35 ug/L 350818 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual) 1 Anthracene-diO- 188 C14D10 001719-06-8 910 2 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 1000215-61-8 33 4 Phenanthrene-diO 188 C14D10 001517-22-2 32 Abundance Scan 3401 (23.062 min): 11576.D (-3394) (-) 1(18 m/z 188.15 ioo.oo%|

5000 80 94 158 22.80 23.00 23.20 23.40

n/z-> 0 | | 43 52 66 ( . ’M’v .'ft ’’ | . J > |'l . 1 I 1 I1!46lll 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 i‘ ‘ “ m/z 94.10 22.18%| Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/ z 80.10 20.31%| 80 94 160 , , 17 30 42 52 66 , 108118 132 146 I. 170179 0 mmTmuTHt — m/z-> 10 2030405060 70 8090 100110120 130140 150160170180190 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188

22.80 23.00 23.20 23.40 5000- m/z 184.10 16.57%| 143 51 64 76 89 102 115 130 |h 158 170 miz-> 0 --------------------- -kryvalpai. 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 I Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11)]tetradeca... . \ , . ................... 188 22.80 23.00 23,20 23.40 m/z 189.10 14.65%|

5000 79 91 55 67

m— 105 191

0 1V 117 158.173 4 TI- .. II,.... 145 —12011101"nr n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11576.D 060302.M Wed Jun 05 12:29:50 2002 Page 14

NYC-WTC_000015579

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NYC-WTC_000015579Source: NYC Law Department, mirrored locally

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