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GCMS analysis results for sample AE10164, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for sample AE10164 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023487–000023501

Folder label: “GCMS X 5/9/02 A 5/13/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\10164.D Vial: 12 Acq On : 13 May 2002 8:27 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.55 ug/L 537550 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 87 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 38 Abundance Scan 3410 (23.115 min): 10164.D (-3403) (-) m/z 188.10 100.00% 188

5000 ..................................................... 94 . 80 160 22.80 23.00 23.20 23.40 — m 44 57 66 132 „ m/z 94.10 25.26% 0- miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d1 0- 188

5000 22.80 23.00 23.20 23.40 m/ Z 184.10 14.03% 80 94 160 . 17 30 42 52 0 | I 108118 132 146 1 170179 0 1 11111111 j 1111 j 11111 j 11 u ] rl I j । j 1111111! ] I 111 [ i iTi [ 11TTTTI । j ] 11 it| 1111111 "I’t 11 > । j 111 tHt’ । ri i- mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 80.00 12.84%

80 94 160 30 42 52 66 0 TPTITWTTMTTTTTTTT 1 t | |I I I I | t I108 J I ] I 118 I I I | J 11 132 I | 1 I H | 146 I I I I | I t’l 1 ’’’ I 179179— m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 22.80 23.00 23.20 23.40 m/z 160.15 11.16%

5000 143 . 89 115 . 51 64 76 | 102 I. 180 ill 158 170 0 ----------------------- --- m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10164.D 050102 .M Tue May 14 11:42:12 2002 Page 8

NYC-WTC_000023499

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NYC-WTC_000023499Source: NYC Law Department, mirrored locally

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