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GCMS analysis results for sample AE10164, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for sample AE10164 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023487–000023501

Folder label: “GCMS X 5/9/02 A 5/13/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\10164.D Vial: 12 Acq On : 13 May 2002 8:27 pm Operator: Mclean Sample : 5/9 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Phenanthrene, 9-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.26 ug/L 250919 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 45 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 4 Phenanthrene, 4-methyl-192 C15H12 000832-64-4 40 Abundance Scan 3319 (22.580 min): 10164.D (-3313) (-) m/z 192.10 100.00% 192

5000

0 -4377 2 4. 118 111111" " ।" 146 160

i" " i" " I ++ ... a .. . 22.20 22.40 22.60 22.80 23.00 m/Z 191.00 19.51% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

----- 5000 22.20 22.40 22.60 22.80 23.00 m/z 146.10 18.28% 96

miz-> 29 39 51 63 75 83 0 11—0211—0001—0000—————31—100————umu—mT’TJrTDWTTTT I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 115 126 139 152 165 176 l— Abundance #80999:5H-Dibenzo[a,d]cycloheptene 192 > 22.20 22.40 22.60 22.80 23.00 177 5000 m/z 193.10 16.52% 165 89 76 ,102 115 128 139 152 | 0 39 51 63 I 1 ' 1 1 1 1 1 "'l 1 " 1 I'1 1 " 1 ,'1'1 ' I ' tl’rmrt!’ 'Uh I'll I I | r’l’i | I I !'l | i I i ir -47 Hl 11‘ mfe—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- -i-r-p-r-r-r-p- ' I ' ' ' ' I 1 ' 192 22.20 22.40 22.60 22.80 23.00 161 m/z 160.10 12.02% 5000-

77 91 121 149 177 52 64 103 138

m/z-> 0 mMM#HHH 1..... I " ‘ 'i' 11 — 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TTpr ......... -..... y, 22.20 22.40 22.60 22.80 23.00

10164.D 050102.M Tue May 14 11:42:10 2002 Page 7

NYC-WTC_000023498

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NYC-WTC_000023498Source: NYC Law Department, mirrored locally

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