GC-MS chromatogram data, sample 11410, May 2002

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Data File : C:\MSDCHEM\1\DATA\051702\11410.D Vial : 19 Acq On : 18 May 2002 4:16 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.30 ug/L 413546 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 7 2 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97-5 45 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 Abundance Scan 3319 (22.580 min): 11410.D (-3311) (-) m/z 192.10 100.00% 192

5000

82 96 146 160 ■ । ' ■ • ■ । 080 22.20 22.40 22.60 22.80 23.00 42 52 0 TITTTTTTTTTTTT । P 111111111 70 82 ,1 l‘l 1111111 p 118 TP# -H 1" i" m/z 191.00 21.13% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 m.... , 22.20 22.40 22.60 22.80 23.00 m/z 193.00 14.07% 96

m/z-> 29 39 51 63 74 83 J Ol 11000—0000000U207T01011111110—nmmOTTuT 115 126 139 152 165 +l TH176 J 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 T-p-r- i Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- 192 164 ,................. ............................... 22.20 22.40 22.60 22.80 23.00 5000 99 m/z 146.00 13.94% 115 47 77 177 67 125 134 146 0 —2738 11157/117 +7++I rlmr ’111 4+155, — T-p-r mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- ........ ...4...... . 192 22.20 22.40 22.60 22.80 23.00 m/ z 96.10 13.77%

5000

96 165 28 39 51 63 74 83 1 105 115 126 139 152 i 176 0 TTTPPTTTTTTTTTTTT TTTTTTTTPTTTTTTTTTTTTH " i11 1 । 1 1 ■ ' । ' ■ ■ । 1 ■ ■ 1 i ' n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

11410.D 050102.M Tue May 21 15:54:24 2002 Page 6

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