GCMS analysis results for sample AE09569, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\050902\9569.D Vial: 24 Acq On : 10 May 2002 10:51 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.35 ug/L 573055 Phenanthranene-dl0 • 22.96

Hit# of

1 Phenanthrene, 5 Tentative ID

9-methyl- 2 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 MW MolForm

192 C15H12 CAS#

000883-20-5 103986-76-1 Qual

53 50 V 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 40 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 Abundance Scan 3319 (22.580 min): 9569. D (-3308) (-) m/z 192.10 100.00% 192

5000

82 96 160 146 ....... A..... A. 22.20 22.40 22,60 22.80 23,00 42 70 122 0 ।।11" ।1"11 ■■ ■■ । ■11 ■ j ■ 11 TmTPhmPT - HTp m/z 191.10 19.54% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

I ______________ / I 5000 ■ i • ■ 1 1 i 1 1 1 1 1 i 1 22.20 22.40 22.60 22.80 23.00 m/z 146.10 17.48%| 96 165

miz-> 29 39 51 63 74 83 I 115 126 139 152 44 176 0- 11" " i " " i" " i ■" ’ i" i ■11 ■ i1 ■' 11 ■11' i" " i" " i11" i" "’i" " I'11" i l argan :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid 161 192 21...... 22,20 22.40 22.60 22.80 23.00 5000 105 m/Z 193.10 15.80%| 77 132 91 . 145

m/z-> 0— I " ' 39 51 m , ' l1 65 ,111 n ' ll. -l+ —— 115 175 ka m U 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842: Phenanthrene, 2-methyl- - 192 22.20 22.40 22.60 22.80 23.00 m/z 96.00 12.74%|

5000

96 27 39 51 82 | 63 115 126 139 152 165 176 . 0 111"11111 ‘‘l " " 11' " I" I T II ''1' i""i" " i"111" "1111' i'i' 1111'th 111 rl 111 i’l II’T - iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9569.D 050102.M Mon May 13 11:45:35 2002 Page 6

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