GCMS analysis results, sample AE12531, June 2002

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Laboratory report showing GCMS analysis results for sample AE12531 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014509–000014531

Folder label: “GCMS X 5/28/02 A 5/29/02”

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NYC 9/11 Public Portal Document library search compound Report Data File : C:\MSDCHEM\1\DATA\052902\12531.D Vial: 22 Acq On : 30 May 2002 3:11 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 13 Phenanthrene, 9-methyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T.

22.54 0.27 ug/L 311516 Phenanthranene- dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 42 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 42 4 Phenanthrene, 4-methyl- 192 C15H12 000832-64-4 42 Abundance Scan 3311 (22.533 min): 12531 .D (-3304) (-) m/z 192.10 100.00% 192

5000 ....... I]........ 22.20 22.40 22.60 22.80 40 52 0- qmpmhptthmnmtmmpmtmm 70 82 %6 118 146 160 J m/z 191.10 17.01% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 m/z 193.10 15.89%I 29 39 51 63 74 83 T 115 126 139 152 165 176 | 0 ■ i“'11• ■ “i““i“i• I■ri■ i11 rh11 ''I'1ITI,n 1111111''1 ‘11'''P1111111'i1 rl i'' Wtt n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125844: Anthracene, 2-methyl- 192

22.20 22.40 22.60 22.80 5000 m/z 160.10 11.70

92 96 165 6374 ll 115 139 150 „| 176 . 0 ।■ 11.. 1111111,1111r> ।! ri > ** i’r 111! > 111 > > 11 ri 1111! i 11111'| 11 > t ■ । i'1'l > 111 11111 ‘ Trrpor n/z-> 2030405060 70 8090 100 110 120130140 150160170 180 190 200 Abundance #125856: Phenanthrene, 1-methyl- 19/2 1— 22.20 22.40 22.60 22.80 m/z 96.00 11.45

5000

96 e 27 39 51 63 82 ll 115 126 139 152 190 178 0- 11 j,,; । , i ,‘I n 11 pi 111111 > q vrri ’ rl'| 1ayenu TT 11 “ 1 > | “ r*’ .... rh 111 i'i'i 11l Ih i . i’l * 1B.I miz-> 20 30 40 50 60 70 80 90 100 110120130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

12531.D 052202.M Mon Jun 03 11:43:16 2002 Page 16

NYC-WTC_000014529

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NYC-WTC_000014529Source: NYC Law Department, mirrored locally

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