GCMS analysis results for sample AE11932, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11932.D Vial: 12 Acq On : 23 May 2002 6:56 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Phenanthrene, 9-methyl- Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

22.54 0.27 ug/L 281690 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 53 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 4 Phenant hrene, 3 -methyl- 192 C15H12 000832-71-3 42 Abundance Scan 3312 (22.539 min): 11932.D (-3299) (-) m/z 192.10 100.00% 192

5000

■ ■ i 1 ■ • * i • ■ _ . 82 96 146 160 22.20 22.40 22.60 22.80

nz-> 0 11111 rp-n 42 11! 111111 > 11 ■ 66 > 1111 ■ I ■ । ! 111111111 ■ ■ 111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 n 111.... । .... । . , I t i l. ।... I'l. I.. j ....p... I1 4 m/z 191.00 20.35% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 m/z 193.10 14.40% 29 39 51 63 74 83 115 126 139 152 165 176 J ) 0 i j 1111 j i n t'| 1111 |'i i i I j i‘i 1111 r i "l’i rh rl ■ l >..■ I 1 ■ rr-rj | .'I1. ■ । ■ rhi । ■i ill* 1 • i * • m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125856: Phenanthrene, 1-methyl- 192

22.20 22.40 22.60 22.80 5000 m/z 146.10 13.48%

96 seE 27 39 51 63 82 1l 115 126 139 152 190 178 0-\ [ r > 111 ■ 11 i-j 1 ■ 1 r|*i i n 11'11111 rn "l’i rh > 1*1 > (> i > i rent 11.. i. (.. rq i... |*l... (i’n . ।. 111,. i i'l* Wttt miz-> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842: Phenanthrene, 2-methyl- ....... i. ii . * I ‘ 1 ‘ ' I 192 22.20 22.40 22.60 22.80 m/z 96.00 12.17%

5000

96 . 27 39 51 63 82 ,| 115 126 13g 152 165 176 O'\ 111 > rp !T|'| 1111 p 11 111'11 | I'l !•> I J-I'i rf | I'l || I 1111 rri 11111111111'| 11111*11111 .'i'l. |.. 1111 . ri' *pr . mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

11932.D 052202.M Wed May 29 09:51:38 2002 Page 19

NYC-WTC_000013690