GCMS analysis results for sample AE06338, May 3 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050102\6338.D Vial: 14 Acq On 1 May 2002 8:18 pm Operator: Mclean Sample re-ext 4/29 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Phenanthrene, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.34 ug/L 373642 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 5 2 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9/ 59 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20/ 53 4 Phenanthrene, 3-methyl- 192 C15H12 000832-7 -3 45 Abundance Scan 3319 (22.580 min): 6338. D (-3312) (-) m/z 192.10 "100.00% 192

5000 ............. / —1 I 1 1 '' I ' 1 1 1 I n 1 11 I 11 1 1 I 1 96 146 160 22.20 22.40 22.60 22.80 23.00 42 52 70 °2 | 118 m/z-> "i... 1... +— ' i IT i I r' |' i F i i j l i > i | i i i i | > ‘ I > | > > ' । | I I I । | । I I । |

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.10 A 18.70% Abundance #125842: Phenanthrene, 2-methyl- 192

nppkn I ( I I kl 1 I I I * I I I I I I I I 5000 22.20 22.40 22.60 22.80 23.00 m/Z 96.10 14.90% 96 ,

m/z-> 27 39 51 63 । । । । । । । । । । । । । । । । । । । । । । >'i । 82 | - *1* 115 126 139 152 165 176 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 , U Abundance #125856: Phenanthrene, 1-methyl- 192 1 । ' 1 1 1 । 1 ' .... I 1 1 I ' ■ ' 1 I 1 22.20 22.40 22.60 22.80 23.00 5000 m/ z 146.10 13.44%

96 27 39 51 63 82 115 126 139 152 165 178 । i’I'i । । । । । । । F| i i i i । i i fi । i'i । । । । rt'rpl i rl‘| rl'I i । TTTTmutttmmi m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 4 22.20 22.40 22.60 22.80 23.00 m/ z 193.00 12.63%

5000

96 165 I 29 39 51 63 74 83 l 115 126 139 152 I 176 [ ,........... 1 ................. i । i i 1 1 । 1 1 1 1 । 1 1 1 1 । 1 i i i । 1' 1 1 > । < i i i |I‘ fli । I I । । । । । । । । । । । । । । > > । । । । F । । । > । |' I । 1 । । 1I1 । । । 1 ri । । । il| T-p-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

6338.D 050102.M Thu May 02 12:23:43 2002 Page 8

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