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GCMS analysis results for sample AE06338, May 3 2002

Machine-extracted title · confidence 100%

Report listing other unknown compounds and surrogate recovery data from GCMS analysis conducted on May 3 2002.

NYC-WTC_000044496–000044509

Folder label: “GCMS X 4/29/02 A 5/1/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050102\6338.D Vial: 14 Acq On 1 May 2002 8:18 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.61 ug/L 669713 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 90- 2 Phenanthrene-diO 188 C14D10 001517-22-2 8.7 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 36 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 Abundance Scan 3409 (23.109 min): 6338.D (-3403) (-) m/z 188.20 100.00% 188

5000

■ 1 । > 1 D । । । । । । । । | i i | ar 80 94 158 22.80 23.00 23.20 23.40 _ 43.466 1 , ....... , 11" | rf- f | । I T f f i i I • ( r r- t . | i i . < | i . I , j i 253 268 7 । । n । । [ n i i । । I i- m/ z 94.10 15.40% m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #79826: Anthracene-d10- 188

5000 T I [ I I I I I I I I I" 22.80 23.00 23.20 23.40 m/z 189.15 14.94% 80 94 -|60 | I । ( | । 28 40 52 66 । । । |i । l'i । ii r 11.106118132146. ...... 1 UTTT I I I I I I I I ' I 1 1 i ■ 1

ti/z->_______ 20 40 60 80 100 1 20 140 160 180 200 220 240 260 Abundance #79827: Phenanthrene-d10 188 1 f । । — । J । । r । । । । — [ । । । । r

22.80 23.00 23.20 23.40 5000 m/z 80.10 12.60%

80 94 160 28 40 52 66 l| 108120132 146 J I Tr -L 1ITTP+TPT 1 1 i ■ 1 ' 1 i 1 1 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #79806: Naphthalene, 2,6-dimethoxy- ' 1 | 1 1 ' 1 | 1 1 ‘ | ' 1 ' 1 | ' ' 188 22.80 23.00 23.20 23.40 173 m/z 184.10 11.87% 145 5000 102 28 114 130 15 | I 51637588, 157 11"/ 1" J ' I 1 1 11 1 1 ‘ 1 T' ' 1 1 i ' 1 11 I ' 1 T”| I 1 i ~ "III It | i i i i | i i T 1 I I 1 > [ I 11 I I I I I I I I I I P m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 22.80 23.00 23.20 23.40

6338.D 050102.M Thu May 02 12:23:43 2002 Page 9

NYC-WTC_000044508

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NYC-WTC_000044508Source: NYC Law Department, mirrored locally

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