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GCMS blank analysis results for sample AE11379, May 21, 2002

Machine-extracted title · confidence 95%

Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.

NYC-WTC_000025054–000025071

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\0515LB.D Vial: 16 Acq On : 18 May 2002 1:49 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Anthracene-dlO- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.34 ug/L 493930 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 91 3 1,4-Naphthoquinone, 2,3-dihydro-... 188 C12H12O2 1000157-22-3 40 4 2,2,9,9-Tetramethyldec-5-ene-3 ,7... 188 C14H20 102745-35-7 38 Abundance Scan 3409 (23.109 min): 0515LB.D (-3403) (-) m/z 188.10 100.00% It®

5000

------ 42 52 64 80 94 132 160 । 22.80 23.00 23.20 23.40 O-T [ " 1' 1111 i; I 11 > [i tt-rp-i H ......... .. I. ■ । .................... ... mH 1i" " r207i'11 rn/z 189.15 16.05% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79826: Anthracene-d1 0- 188

5000 ■ ■ । । ■ I ■ ■ ‘ ■ i ■ । । । । ■ i 22.80 23.00 23.20 23.40 m/z 184.10 15.03% ee 80 94 160 17 30 42 52 °0 108118 132 146 1 170 0 TTTTWTTTTTpmpmo ■I‘ "1 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79827: Phenanthrene-d10 108

22.80 23.00 23.20 23.40 5000 m/z 94.10 10.33%

80 94 160 30 42 52 66 108118 132 146 1 170 , 0 1111111'11T ITTTT+TTFr nt I I 1-1 ] l ! I t | "I11"..... ... ■ 'I ।11111" ■ i ",|||T" " r1'1'1 'T1 r ‘" r " ' i1" m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79805:1,4-Naphthoquinone, 2,3-dihydro-5,8-dimethyl- 188 22.80 23.00 23.20 23.40 173 m/z 80.10 10.17%

5000 145 82 91 159

27 39 51 65 105 115 131

m/z-> 0 --+++++ HHL, HH L 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 22.80 23.00 23.20 23.40

0515LB.D 050102.M Tue May 21 11:58:14 2002 Page 7

NYC-WTC_000025064

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NYC-WTC_000025064Source: NYC Law Department, mirrored locally

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