GCMS analysis results, sample AE09154, May 2002

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GCMS analytical report for environmental sample AE09154 including surrogate compound data from May 15, 2002.

NYC-WTC_000022819–000022849

Folder label: “GCMS X 5/8/02 A 5/10/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\DATA\050902\9154 .D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene-dlO- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.51 ug/L 580060 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 83 3 1,4-Naphthoquinone, 2,3-dihydro-... 188 C12H1202 1000157-22-3 38 4 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 37 Abundance Scan 3409 (23.109 min): 9154.D (-3402) (-) m/z 188.10 100.00% 188

5000 94 /.................................... 160 ■ 1 i 1 1 1 ■ i 1 1 1 ' i ■ ■ 1 ' । 1 1 1 ■ i „ 80 22.80 23.00 23.20 23.40

n/z-> 0 +43, 57, - lul.+ 207 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 ‘I* "’'I' m/ z 94.05 21.83% Abundance #79826: Anthracene-d1 0- 188

.................................... ................. 5000 22.80 23.00 23.20 23.40 m/z 189.10 16.77% 17 30 42 52 ee 66 . 80 94 160 108118 132 146 I 170 |.i 0 I''''I'1'' 111 " 111111 ■1111'11'I'11111 T—tth m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79827: Phenanthrene-d10 18 8

22.80 23.00 23.20 23.40 5000 m/z 160.10 14.85% ft 801 94 160 30 42 52 11 66 108118 132 146 1 170 | 0 mmmPTHTtmI tap/VAnnyunnslanoyuatynhazayennzt ' i" ■ ‘i" ■ m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79805:1,4-Naphthoquinone, 2,3-dihydro-5,8-dimethyl- ............ ................................... 188 22.80 23.00 23.20 23.40 173 m/ z 80.10 13.59%

5000 145 82 91 159 65 115 .. 131 27 39 51 105 0 -++4++H+HH — lzaryphjarr — TTTgm)ut 4 Ti r —T- । । । n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 22.80 23.00 23.20 23.40

9154.D 050102.M Mon May 13 11:28:52 2002 Page 10

NYC-WTC_000022833

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