GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\060702\12739.D Vial: 15 Acq On 7 Jun 2002 7:58 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 17 Anthracene-dlO- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T. 23.06 0.38 ug/L 456510 Phenant hranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 87 2 Phenanthrene-diO 188 C14D10 001517-22-2 86 3 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 40 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 Abundance Scan 3401 (23.062 min): 12739.D (-3394) (-) m/z 188.10 100.00% 188

5000

----- 80 94 42 52 66 132 158 22.80 23.00 23.20 23.40 0 mopthnptmpt '“ill..| Tt n I 11 I 11111 [TT Tot 1mn m/z 189.10 18.35% miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 18 8

\ . .......... 5000 22.80 23.00 23.20 23.40 m/z 80.10 13.82% ee 80 94 160 , .

miz-> 17 30 42 52 ° J J 108118 132 0- I'111111 “ 1 ■■ “ 11 ■■ ■ 111 “ i111' i “1111 “1111'111 ■■11 “'' i''' '.|111' 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 146—4.179179 4 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 13.42%

94 80 160 30 42 52 66 miz-> ,| 108118 132 146 11, o1TTTIWIWWTTWTTHTTTHT I 1 | I I I I | I 1 I I | I I J I ) I I । I | l t H | > I t-l-pi fl,P|,i | 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 179179,1 Abundance. #79716: -(4-Tolyl)-3-methyl-pyrazol-5-one - its 22.80 23.00 23.20 23.40 91 m/z 94.00 12.92% 105 5000 119 65 — ... 41 51. .7 Hr 0 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ “ ■ i ■"' i ■ ■" i ’’’ ■ ।" ■11 ■ ■ ■ 'I 146 TIUTTPTTTTITTTTT i ■1111 1. • ■ i ■ ■ ■ ' I 1 ■ i । 1 1 ' 1 1 1 । 1 nfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12739.D Q60302.M Mon Jun 10 11:51:16 2002 Page 20

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