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GCMS analysis results for sample AE07975, April 18, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07975 conducted on April 18, 2002.

NYC-WTC_000047577–000047592

Folder label: “GCMS X 4/4/02 A 4/15/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020415\07975.D Vial: 15 Acq On 15 Apr 2002 10:15 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Anthracene-d10- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.40 ug/L 539020 Phenanthranene- dl 0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 91 Phenanthrene-dl0 188 C14D10 001517-22-2 64 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 47 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 37 Abundance Scan 3420 (23.174 min): 07975.D (-3413) (-) m/z 188.40 100.00% 14 8

5000

‘TT 40 52 66 80 94 1 32 1 46 158 I 22 80 2300 23.20 23.40 23 60 o mmmmm-p--mmmmmmmmmmmmmm ■ । ■"1 T‘‘T m/z 189.40 18.00% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 108

5000 22.80 23 00 23 20 23.40 23.60 m/z 94.25 12.64% rr 80 94 160 17 30 42 52 ° | I 102 118 132 146 | 170 1801, 0 ITTr l"i ri»|i ri 1111111111!; 11111»»111 n 11 11111111 h । ti 11 i t 11111»111 n 111 ........... । > ii | pPr TTur n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827 Phenanthrene-d10 168

l-rT •IBnnTr 22 80 23 00 23.20 23.40 23.60 5000 m/z 184.35 12.19% | 80 94 160 30 42 52 66 n/z-> 0 1 102110118 132 146 TTTTTTHt l |■ I" "I ■ ■" 1111 ■ I ■■ i ■ I ■ r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 +7019. — Abundance #79716: -(4-Tolyl)-3-methyl-pyrazok 5-one TII 168 22 80 23 00 23 20 23.40 23.60 91 m/z 80.30 9.92% 105 5000 119 65 — 0^p 41 51.. . 146 1+ 11 ”l' 11"111"' I r ''I' r 111 r ''' i " '11 ■ ‘ II’T L • i 1 ■ ■ ■ i /z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23 00 23.20 23 40 23.60

07975.D 041202SCAN.M Tue Apr 16 13:45:22 2002 Page 11

NYC-WTC_000047591

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